5-Bromoisoquinoline
- CAS No.
- 34784-04-8
- Chemical Name:
- 5-Bromoisoquinoline
- Synonyms
- 5-BromoisoquinoL;AKOS BBS-00003132;BUTTPARK 44\07-76;5-BROMOISOQUINOLINE;5-Bromo Isoquinolin;Isoquinoline, 5-bromo-;5-Bromoisoquinoline,97%;5-Bromoisoquinoline,98%;5-Bromoisoquinoline >5-Bromoisoquinoline, HCl
- CBNumber:
- CB3135741
- Molecular Formula:
- C9H6BrN
- Molecular Weight:
- 208.05
- MDL Number:
- MFCD01646405
- MOL File:
- 34784-04-8.mol
- MSDS File:
- SDS
Melting point | 83-87 °C (lit.) |
---|---|
Boiling point | 95-97°C 0,1mm |
Density | 1.564±0.06 g/cm3(Predicted) |
Flash point | 95-97°C/0.1mm |
storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
solubility | Chloroform, Dichloromethane, Ethyl Acetate, Methanol |
pka | 4.39±0.13(Predicted) |
form | Solid |
color | Yellow |
BRN | 114468 |
InChI | InChI=1S/C9H6BrN/c10-9-3-1-2-7-6-11-5-4-8(7)9/h1-6H |
InChIKey | CYJZJGYYTFQQBY-UHFFFAOYSA-N |
SMILES | C1C2=C(C(Br)=CC=C2)C=CN=1 |
CAS DataBase Reference | 34784-04-8(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS07 |
|||||||||
---|---|---|---|---|---|---|---|---|---|---|
Signal word | Warning | |||||||||
Hazard statements | H315-H319-H335 | |||||||||
Precautionary statements | P261-P264-P271-P280-P302+P352-P305+P351+P338 | |||||||||
Hazard Codes | Xi,Xn | |||||||||
Risk Statements | 36/37/38-21/22-20/21/22 | |||||||||
Safety Statements | 26-36-36/37/39 | |||||||||
WGK Germany | 3 | |||||||||
Hazard Note | Irritant | |||||||||
HS Code | 29334900 | |||||||||
NFPA 704 |
|
5-Bromoisoquinoline price More Price(42)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich | 594261 | 5-Bromoisoquinoline 98% | 34784-04-8 | 1g | $25 | 2023-01-07 | Buy |
Sigma-Aldrich | 594261 | 5-Bromoisoquinoline 98% | 34784-04-8 | 5g | $29 | 2023-01-07 | Buy |
TCI Chemical | B3313 | 5-Bromoisoquinoline >96.0%(GC)(T) | 34784-04-8 | 1g | $38 | 2024-03-01 | Buy |
TCI Chemical | B3313 | 5-Bromoisoquinoline >96.0%(GC)(T) | 34784-04-8 | 5g | $111 | 2024-03-01 | Buy |
Alfa Aesar | L19632 | 5-Bromoisoquinoline, 98% | 34784-04-8 | 1g | $60.4 | 2021-12-16 | Buy |
5-Bromoisoquinoline Chemical Properties,Uses,Production
Description
5-
Chemical Properties
White to yellow-brown crystals
Uses
Starting material employed in palladium-catalyzed aminomethylation and amination reactions.
Synthesis Reference(s)
[1] W. Brown, A. Gouliaev. “Bromination of Isoquinoline, Quinoline, Quinazoline and Quinoxaline in Strong Acid.” ChemInform 98 1 (2002).
Synthesis
To mechanically stirred concd H2SO4 (42.5 mL) at 0 °C, isoquinoline (1; 5 mL, 42.5 mmol) was slowly added. The mixture was cooled to –25 °C, and NBS (9.83 g, 55.2 mmol) was added at such a rate that the reaction temperature was kept between –25 °C and –22 °C. The mixture was stirred at -22±1 °C for 2 h and at -18±1 °C for 3h. The mixture was then worked up as described above to give 6.16 g (72%) as a slightly off-white solid after chromatography; mp 81–82 °C. The solid was further purified by sublimation (75 °C/0.2 mmHg) to give 5-Bromoisoquinoline as a white powder[1].
5-Bromoisoquinoline Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Changzhou Jiuwu Chemical co., Ltd. | +86-0519-85121086 +8613775162768 | info@jiuwuchem.cn | China | 75 | 58 |
Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 | sales@capotchem.com | China | 29798 | 60 |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 16914 | 58 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29894 | 58 |
Changzhou Ansciep Chemical Co., Ltd. | +86 519 86305871 | sales@ansciepchem.com | CHINA | 4242 | 58 |
Accela ChemBio Inc. | +1-858-6993322 | info@accelachem.com | United States | 19343 | 58 |
Hubei xin bonus chemical co. LTD | 86-13657291602 | linda@hubeijusheng.com | CHINA | 22968 | 58 |
Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | sales@chemdad.com | China | 39916 | 58 |
Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63711 | 58 |
Wuhan Chemwish Technology Co., Ltd | 027-67849912 | sales@chemwish.com | CHINA | 10828 | 58 |
View Lastest Price from 5-Bromoisoquinoline manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
![]() |
2021-10-14 | 5-Bromoisoquinoline
34784-04-8
|
US $10.00 / KG | 1KG | 99% | 20 tons | Hebei Zhanyao Biotechnology Co. Ltd | |
![]() |
2021-08-05 | 5-Bromoisoquinoline
34784-04-8
|
US $1.10 / g | 1g | 99.00% | 100 Tons min | Dideu Industries Group Limited | |
![]() |
2019-07-06 | 5-Bromoisoquinoline
34784-04-8
|
US $1.00 / kg | 1kg | 99% | 200kg | Career Henan Chemical Co |
-
- 5-Bromoisoquinoline
34784-04-8
- US $10.00 / KG
- 99%
- Hebei Zhanyao Biotechnology Co. Ltd
-
- 5-Bromoisoquinoline
34784-04-8
- US $1.10 / g
- 99.00%
- Dideu Industries Group Limited
-
- 5-Bromoisoquinoline
34784-04-8
- US $1.00 / kg
- 99%
- Career Henan Chemical Co
34784-04-8(5-Bromoisoquinoline)Related Search:
1of4