Methyl 3-amino-4-chlorobenzoate
- CAS No.
- 40872-87-5
- Chemical Name:
- Methyl 3-amino-4-chlorobenzoate
- Synonyms
- Intedanib Impurity 5;Methyl 3-Amino-4-chlorobenzene;METHYL 3-AMINO-4-CHLOROBENZOATE;METHYL, 4-CHLORO-3-AMINOBENZOATE;Methyl3-Amino-4-chlorobenzoate>3-amino-4-chloro-2-methylbenzoate;Amino chlorobenzoic acid methyl ester;3-AMINO-4-CHLOROBENZOIC ACID METHYL ESTER;Methyl 3-AMino-4-chlorobenzoate, 98.0%(GC&T;Benzoic acid, 3-aMino-4-chloro-, Methyl ester
- CBNumber:
- CB3211933
- Molecular Formula:
- C8H8ClNO2
- Molecular Weight:
- 185.61
- MDL Number:
- MFCD03470533
- MOL File:
- 40872-87-5.mol
- MSDS File:
- SDS
Melting point | 83 °C |
---|---|
Boiling point | 292.1±20.0 °C(Predicted) |
Density | 1.311±0.06 g/cm3(Predicted) |
storage temp. | Keep in dark place,Inert atmosphere,Room temperature |
form | crystalline powder |
pka | 1.51±0.10(Predicted) |
color | Pale lemon/gold |
CAS DataBase Reference | 40872-87-5(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
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Signal word | Warning | |||||||||
Hazard statements | H315-H319 | |||||||||
Precautionary statements | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 | |||||||||
Hazard Codes | Xi | |||||||||
HS Code | 2916399090 | |||||||||
NFPA 704 |
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Methyl 3-amino-4-chlorobenzoate price More Price(29)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
TCI Chemical | M1778 | Methyl 3-Amino-4-chlorobenzoate >98.0%(GC)(T) | 40872-87-5 | 5g | $54 | 2024-03-01 | Buy |
TCI Chemical | M1778 | Methyl 3-Amino-4-chlorobenzoate >98.0%(GC)(T) | 40872-87-5 | 25g | $181 | 2024-03-01 | Buy |
TRC | M328668 | Methyl 3-Amino-4-chlorobenzoate | 40872-87-5 | 500mg | $65 | 2021-12-16 | Buy |
Apolloscientific | OR2041 | Methyl 3-Amino-4-chlorobenzoate | 40872-87-5 | 25g | $58 | 2021-12-16 | Buy |
SynQuest Laboratories | 4658-5-X6 | Methyl 3-amino-4-chlorobenzoate | 40872-87-5 | 25g | $64 | 2021-12-16 | Buy |
Methyl 3-amino-4-chlorobenzoate Chemical Properties,Uses,Production
Synthesis
To a solution of 3-amino-4-chlorobenzoic acid (15.0 g, 88.0 mmol) in methanol (90.0 mL), thionyl chloride (13.0 mL) was added drop-wise at 0 °C. The resulting mixture was refluxed for 12h. After completion of the reaction, the reaction mixture was concentrated under reduced pressure. The residue was diluted with water (150 mL) and extracted with ethyl acetate. The organic layer was washed with sodium bicarbonate (50 mL) and brine solution (50 mL) and dried over sodium sulfate. The organic layer was removed under a rotary evaporator to yield Methyl 3-amino-4-chlorobenzoate (15.0 g, 92.5 per cent) as an off-white solid. 1H NMR (400 MHz, CDC13) δ 3.88 (s, 3H), 4.26 (brs, 2H), 7.29 (d, J = 8.2 Hz, 1H), 7.34-7.37 (dd, J = 1.9, 8.2 Hz, 1H), 7.45 (d, J = 1.9 Hz, 1H).
Methyl 3-amino-4-chlorobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Capot Chemical Co.,Ltd. | +86-(0)57185586718 +86-13336195806 | sales@capot.com | China | 29791 | 60 |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18779 | 58 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32957 | 60 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29884 | 58 |
Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | sales@chemdad.com | China | 39894 | 58 |
Wuhan Chemwish Technology Co., Ltd | 027-67849912 | sales@chemwish.com | CHINA | 10821 | 58 |
CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49374 | 58 |
Antai Fine Chemical Technology Co.,Limited | 18503026267 | info@antaichem.com | CHINA | 9636 | 58 |
Xi'an Yutbon Pharmaceutical Technology Co., Ltd | 029-81140587 +8618717328141 | sales@yutbon.com | China | 454 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34553 | 58 |
View Lastest Price from Methyl 3-amino-4-chlorobenzoate manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2019-07-06 | methyl 3-amino-4-chlorobenzoate
40872-87-5
|
US $7.00 / kg | 1kg | 99% | 100kg | Career Henan Chemical Co |
- methyl 3-amino-4-chlorobenzoate
40872-87-5
- US $7.00 / kg
- 99%
- Career Henan Chemical Co
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