DIBUTYLCARBAMYL CHLORIDE
- CAS No.
- 13358-73-1
- Chemical Name:
- DIBUTYLCARBAMYL CHLORIDE
- Synonyms
- tl459;Brn 2040828;Einecs 236-410-3;DIBUTYLCARBAMYL CHLORIDE;dibutylcarbamoylchloride;dibutyl-carbamoylchlorid;dibutylcarbamic chloride;1,6-dibutyl-carbamicchlorid;Carbamoyl chloride, dibutyl-;Dibutylcarbamic acid chloride
- CBNumber:
- CB3783443
- Molecular Formula:
- C9H18ClNO
- Molecular Weight:
- 191.7
- MDL Number:
- MFCD00015740
- MOL File:
- 13358-73-1.mol
- MSDS File:
- SDS
| Boiling point | 257-260 °C(lit.) |
|---|---|
| Density | 0.985 g/mL at 25 °C(lit.) |
| refractive index |
n |
| Flash point | 110 °C |
| pka | -1.85±0.70(Predicted) |
| EWG's Food Scores | 1 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS05 |
|---|---|
| Signal word | Danger |
| Hazard statements | H314 |
| Precautionary statements | P260-P264-P280-P301+P330+P331-P303+P361+P353-P363-P304+P340-P310-P321-P305+P351+P338-P405-P501 |
| Hazard Codes | C |
| Risk Statements | 34 |
| Safety Statements | 26-36/37/39-45 |
| RIDADR | UN 3265 8/PG 3 |
| WGK Germany | 3 |
| RTECS | FD2230000 |
| HazardClass | IRRITANT |
DIBUTYLCARBAMYL CHLORIDE price More Price(6)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Biosynth Carbosynth | FD125484 | Dibutylcarbamic chloride | 13358-73-1 | 250mg | $85 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FD125484 | Dibutylcarbamic chloride | 13358-73-1 | 500mg | $150 | 2021-12-16 | Buy |
| Matrix Scientific | 065822 | Dibutylcarbamic chloride | 13358-73-1 | 500mg | $237 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FD125484 | Dibutylcarbamic chloride | 13358-73-1 | 1g | $255 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FD125484 | Dibutylcarbamic chloride | 13358-73-1 | 2g | $434 | 2021-12-16 | Buy |
DIBUTYLCARBAMYL CHLORIDE Chemical Properties,Uses,Production
Uses
It is reported that Dibutylcarbamoyl Chloride is used as a reagent for the preparation of 7-azaindole-1,3-dicarboxamide hydroxyethylamine which exhibited potent BACE-1 enzyme inhibition. Also it is used for the preparation of copper salicylaldehyde semicarbazone complex which showed cytotoxicity in human cancer cells.
Preparation
In a 100 mL roundbottomed flask were placed dibutylamine (6.45 g, 0.05 mol), pyridine (4.0 g, 0.05 mol), N-cyclohexyl-N0,N0,N00,N00-tetraethylguanidine (12.7 g, 0.05 mol), and toluene (40 mL). The resulting solution was cooled to 10 °C using an ice/salt bath and carbon dioxide was bubbled into the cooled solution for 30 min. After this period of time, the pre-formed carbamate solution was added in a single portion via a cannula to a cooled ( 10 °C) solution of thionyl chloride (6 g, 0.05 mol) in toluene (40 mL). The reaction mixture was stirred at 10 °C for 45 min. It was then poured into 0.1 m aq. HCl (100 mL), giving rise to two layers. The organic layer was separated, dried over anhydrous Mg2SO4, filtered, and the solvent was removed in vacuo. The residue was distilled in vacuo (1 mmHg) at 95–98 °C to give 7.62 g (79%) of N,N-dibutyl carbamoyl chloride.
DIBUTYLCARBAMYL CHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
DIBUTYLCARBAMYL CHLORIDE Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49374 | 58 |
| Shaanxi Dideu Medichem Co. Ltd | +86-29-87569262 +86-15319487004 | 1015@dideu.com | China | 2127 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
| Meryer (Shanghai) Chemical Technology Co., Ltd. | 021-61259108 18621169109 | market03@meryer.com | China | 40228 | 62 |
| Energy Chemical | 021-021-58432009 400-005-6266 | sales8178@energy-chemical.com | China | 44688 | 61 |
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42958 | 64 |
| Hangzhou Yuhao Chemical Technology Co., Ltd | 0571-82693216 | info@yuhaochemical.com | China | 9387 | 52 |
| Chengdu Ai Keda Chemical Technology Co., Ltd. | 4008-755-333 18080918076 | 800078821@qq.com | China | 9718 | 55 |
| Chengdu HuaXia Chemical Reagent Co. Ltd | 400-1166-196 13458535857 | cdhxsj@163.com | China | 13350 | 58 |
| Shandong Nayazuo Chemical Technology Co. LTD | 400-873-6778 18660992876 | 3584419101@qq.com | China | 4970 | 58 |
View Lastest Price from DIBUTYLCARBAMYL CHLORIDE manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-02-26 | Dibutylcarbamyl chloride
13358-73-1
|
US $0.00-0.00 / KG | 1KG | 99.0%+ | 100 tons | Shaanxi Dideu Medichem Co. Ltd |
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- Dibutylcarbamyl chloride
13358-73-1
- US $0.00-0.00 / KG
- 99.0%+
- Shaanxi Dideu Medichem Co. Ltd