5,10-tetraMethylindeno[2,1-a]indene
- CAS No.
- 89057-44-3
- Chemical Name:
- 5,10-tetraMethylindeno[2,1-a]indene
- Synonyms
- 5,10-tetraMethylindeno[2,1-a]indene;1,2,5,10-Tetramethylindeno[2,1-a]indene;5,5,10,10-tetramethyl-Inden[2,1-a]Indene;5,5,10,10-tetramethylindeno[2,1-a]indene;5,5,10,10-TetraMethyl-5,10-dihydroindeno<2,1-a>inden;5,5,10,10-Tetramethyl-5,10-dihydroindeno[2,1-a]indene;Indeno[2,1-a]indene, 5,10-dihydro-5,5,10,10-tetramethyl-
- CBNumber:
- CB62640396
- Molecular Formula:
- C20H20
- Molecular Weight:
- 260.37
- MDL Number:
- MFCD26403658
- MOL File:
- 89057-44-3.mol
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H317-H319 |
Precautionary statements | P280-P305+P351+P338 |
5,10-tetraMethylindeno[2,1-a]indene price
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
American Custom Chemicals Corporation | CHM0390496 | 5,5,10,10-TETRAMETHYL-5,10-DIHYDROINDENO[2,1-A]INDENE 95.00% | 89057-44-3 | 5MG | $496.41 | 2021-12-16 | Buy |
AK Scientific | 5743CU | 5,5,10,10-Tetramethyl-5,10-dihydroindeno[2,1-a]indene | 89057-44-3 | 1g | $1835 | 2021-12-16 | Buy |
Crysdot | CD43000055 | 5,5,10,10-Tetramethyl-5,10-dihydroindeno[2,1-a]indene 95+% | 89057-44-3 | 1g | $1129 | 2021-12-16 | Buy |
Alichem | 89057443 | 5,5,10,10-Tetramethyl-5,10-dihydroindeno[2,1-a]indene | 89057-44-3 | 1g | $1244.16 | 2021-12-16 | Buy |
Arctom | SY148053 | 5,5,10,10-Tetramethyl-5,10-dihydroindeno[2,1-a]indene ≥95% | 89057-44-3 | 1g | $1315 | 2021-12-16 | Buy |
5,10-tetraMethylindeno[2,1-a]indene Chemical Properties,Uses,Production
Synthesis
![INDENO[2,1-A]INDENE,5,10-DIHY](/CAS/GIF/6543-29-9.gif)
6543-29-9

74-88-4
![5,10-tetraMethylindeno[2,1-a]indene](/CAS/GIF/89057-44-3.gif)
89057-44-3
At about -78 °C, 2.04 g (10 mmol) of 5,10-tetrahydrodianaphthene (Intermediate I-3) and 37.5 mL (60 mmol) of n-butyllithium (1.60 M hexane solution) were gradually reacted in tetrahydrofuran. Subsequently, 3.8 mL (60 mmol) of iodomethane was added and the reaction mixture was stirred at room temperature for about 3 hours. Upon completion of the reaction, 5 mL of aqueous 1N hydrochloric acid was added to the mixture to quench the reaction. The organic phase was separated and the aqueous phase was extracted with dichloromethane (2 x 100 mL). The organic phases were combined and dried over magnesium sulfate, followed by evaporation of the solvent. The residue was separated and purified by silica gel column chromatography to afford 2.03 g of 5,10-tetramethyldiindene (Intermediate I-4) in 78% yield. The compound was characterized by mass spectrometry/fast atom bombardment mass spectrometry (MS/FAB). The calculated molecular weight of the molecular formula C20H20 was 260.37 and the measured value was 260.45.
References
[1] Patent: US2014/27721, 2014, A1. Location in patent: Paragraph 0127; 0131
[2] Patent: KR2016/56315, 2016, A. Location in patent: Paragraph 0197; 0198; 0205; 0206
[3] Patent: US9537104, 2017, B2. Location in patent: Page/Page column 77; 78; 79
[4] Patent: US2017/12205, 2017, A1. Location in patent: Paragraph 0223; 0230;0321
5,10-tetraMethylindeno[2,1-a]indene Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 | info@spring-chem.com | China | 2068 | 57 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10406 | 58 |
Career Henan Chemica Co | +86-0371-86658258 +8613203830695 | laboratory@coreychem.com | China | 30230 | 58 |
Hefei Hirisun Pharmatech Co., Ltd | +8615056975894 | shawn@hirisunpharm.com | CHINA | 9911 | 58 |
Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52846 | 58 |
CD Chemical Group Limited | +8615986615575 | info@codchem.com | China | 20342 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25356 | 58 |
Coresyn Pharmatech Co., Ltd. | +86-571-86626709 +86-18157142896 | cbc@coresyn.com | China | 9984 | 58 |
PT CHEM GROUP LIMITED | +86-85511178; | peter68@ptchemgroup.com | China | 35425 | 58 |