ChemicalBook >> CAS DataBase List >>2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester

2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester

2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester structure

CAS No.: 6900-93-2

Chemical Name:: 2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester

Synonyms: Lyconnotine;2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester

CBNumber:: CB72306073

Molecular Formula:: C17H25NO3

Molecular Weight:: 291.3853

MDL Number:

MOL File:: 6900-93-2.mol

Last updated:2023-05-04 17:34:41

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2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester Properties

Melting point	123°C
solubility	Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
form	powder
color	Yellow

2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester Chemical Properties,Uses,Production

Description

A minor constituent of Lycopodium annotinum, this alkaloid has [α]¹⁸_D+ 125° and yields an ultraviolet spectrum in EtOH having a single absorption maximum at 235 mJ.1. It yields a crystalline picrolonate, m.p. 230-1 °C. The structure has been determined from the mass spectrum and by comparison with other Lycopodium alkaloids.

Definition

ChEBI: Lyconnotine is a citraconoyl group.

References

Anet et al., Tetrahedron Lett., 751 (1964)
Valenta et al., J. Amer. Chem. Soc., 86,2533 (1964)

2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

2,3,5,9,10,10a-Hexahydro-10-hydroxy-α-methyl-1H,10bH-benzo[ij]quinolizine-10b-propionic acid methyl ester Lyconnotine 6900-93-2