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DEUTERIUM HYDRIDE

CAS No.
13983-20-5
Chemical Name:
DEUTERIUM HYDRIDE
Synonyms
Hydrogen-d1;Hydrogen (D);Hydrogen (1D);(1H,2H)Hydrogen;Einecs 237-773-0;DEUTERIUM HYDRIDE;Hydrogendeuteride;Hydrogenated deuterium;DEUTERIUM HYDRIDE (D, 97%);Deuterium, mol. with hydrogen
CBNumber:
CB8108692
Molecular Formula:
DH
Molecular Weight:
3.02
MDL Number:
MFCD04126430
MOL File:
13983-20-5.mol
MSDS File:
SDS
Last updated:2023-10-17 17:11:58

DEUTERIUM HYDRIDE Properties

Melting point −259.2 °C(lit.)
Boiling point −252.8 °C(lit.)
vapor density 0.07 (21 °C, vs air)
form gas
color colorless

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictogramsGHS hazard pictograms
GHS02,GHS04
Signal word  Danger
Hazard statements  H220-H280
Precautionary statements  P210-P377-P381-P410+P403
Hazard Codes  F+
Risk Statements  12
Safety Statements  16-33-36-38-9
RIDADR  UN 1049 2.1
WGK Germany  3
Autoignition Temperature 1060 °F

DEUTERIUM HYDRIDE price More Price(4)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 488690 Deuterium hydride extent of labeling: 96mol% DH, 98 atom % D 13983-20-5 1l $326 2024-03-01 Buy
Sigma-Aldrich 488690 Deuterium hydride extent of labeling: 96mol% DH, 98 atom % D 13983-20-5 5l $950 2024-03-01 Buy
American Custom Chemicals Corporation RDL0001741 DEUTERIUM HYDRIDE 95.00% 13983-20-5 1L $6582.35 2021-12-16 Buy
American Custom Chemicals Corporation RDL0001741 DEUTERIUM HYDRIDE 95.00% 13983-20-5 5L $7024.71 2021-12-16 Buy
Product number Packaging Price Buy
488690 1l $326 Buy
488690 5l $950 Buy
RDL0001741 1L $6582.35 Buy
RDL0001741 5L $7024.71 Buy

DEUTERIUM HYDRIDE Chemical Properties,Uses,Production

Chemical Properties

col gas [CRC10]Density, g/L: 0.123 [CRC10]

Definition

ChEBI: Deuterium atom is the stable isotope of hydrogen with relative atomic mass 2.014102 and a natural abundance of 0.0115 atom percent (from Greek deltaepsilonupsilontauepsilonrhoomicronnu, second). It contains a deuteron.

Synthesis

About 150 ml. of n-butyl ether, dried over Na, is distilled into the reaction flask and 5.75 g. of LiAlH4 (40% excess) is then added under a nitrogen blanket. The mixture is frozen with liquid N s. The apparatus is then evacuated, and the flask contents are brought to boiling by careful heating. After 1.5 hours, it is again cooled with liquid Ns , the evacuation is repeated, and 5 ml. of 99.5% D2O is added to the solidified mixture, using a hypodermic syringe to pierce the rubber cap. Because of the low reaction temperature, the flask becomes coated with ice on the outside. By repeated immersion in liquid N3, the temperature is controlled so that the ice on the outer wall of the flask does not melt. As soon as the reaction subsides somewhat, two additional portions of 6.5 ml. of DSO each are added (for a total of 18 ml. or 150% excess). The yield is 10 liters of HD. The purity is 97-99%.
LiAlH4 + 4D2O = LiOD + Al(OD)3 + 4HD

DEUTERIUM HYDRIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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(1H,2H)Hydrogen Deuterium, mol. with hydrogen Hydrogen-d1 Hydrogendeuteride DEUTERIUM HYDRIDE DEUTERIUM HYDRIDE, 98 ATOM % D Hydrogen (1D) Hydrogen (D) Einecs 237-773-0 DEUTERIUM HYDRIDE (D, 97%) DEUTERIUM HYDRIDE ISO 9001:2015 REACH Hydrogenated deuterium 13983-20-5 DH Stable Isotopes BioChemical Alphabetical Listings Alphabetical Listings Chemical Synthesis Compressed and Liquefied GasesStable Isotopes DAlternative Energy Deuterated MaterialsStable Isotopes Gases Materials for Hydrogen Storage Synthetic Reagents