Diethyl 2,6-pyridinedicarboxylate
- CAS No.
- 15658-60-3
- Chemical Name:
- Diethyl 2,6-pyridinedicarboxylate
- Synonyms
- Nsc78907;RARECHEM AL BI 0203;DIETHYL DIPICOLINATE;pyridine-2,6-dicarboxyL;2,6-Dicarbethoxypyridine;DIPICOLINIC ACID DIETHYL ESTER;DIETHYL 2,6-PYRIDINEDICARBOXYLATE;diethyl pyridine-2,6-dicarboxylate;Diethyl pyridine-1,6-dicarboxylate;Diethyl2,6-Pyridinedicarboxylate>
- CBNumber:
- CB8150484
- Molecular Formula:
- C11H13NO4
- Molecular Weight:
- 223.23
- MDL Number:
- MFCD00033792
- MOL File:
- 15658-60-3.mol
Melting point | 44°C |
---|---|
Boiling point | 188 °C / 12mmHg |
Density | 1.165±0.06 g/cm3(Predicted) |
storage temp. | Inert atmosphere,Room Temperature |
form | powder to crystal |
pka | -0.20±0.10(Predicted) |
color | White to Light yellow to Light orange |
CAS DataBase Reference | 15658-60-3(CAS DataBase Reference) |
FDA UNII | NS92Z2IS34 |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H315-H319 |
Precautionary statements | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 |
Risk Statements | 36/37/38 |
Safety Statements | 26-36/37/39 |
HS Code | 29333990 |
Diethyl 2,6-pyridinedicarboxylate price More Price(25)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
TCI Chemical | P1240 | Diethyl 2,6-Pyridinedicarboxylate min. 98.0 % | 15658-60-3 | 5G | $78 | 2024-03-01 | Buy |
TCI Chemical | P1240 | Diethyl 2,6-Pyridinedicarboxylate >98.0%(GC)(T) | 15658-60-3 | 25g | $219 | 2024-03-01 | Buy |
TRC | D444763 | Diethyl 2,6-Pyridinedicarboxylate | 15658-60-3 | 500mg | $65 | 2021-12-16 | Buy |
Biosynth Carbosynth | FD67424 | Diethyl 2,6-pyridinedicarboxylate | 15658-60-3 | 25g | $65 | 2021-12-16 | Buy |
AK Scientific | J98984 | Diethylpyridine-2,6-dicarboxylate | 15658-60-3 | 25g | $70 | 2021-12-16 | Buy |
Diethyl 2,6-pyridinedicarboxylate Chemical Properties,Uses,Production
Chemical Properties
Yellow to red crystalline powder
Synthesis
Pyridine-2,6-dicarboxylic acid (10.0g, 59.9mmol) was added into ethanol (120mL),
then 3 drops of concentrated sulfuric acid were added. The mixture was heated to
reflux for 8 hours. After evaporation of the solvent, the solid residue was washed with
saturated Na2CO3 aqueous solution and extracted with chloroform for 3 times. The
organic phase was dried with small amount of MgSO4. The solvent was removed to
afford 1 as white powder (12.6g, 56.3mmol, yield = 94%). 1
H-NMR (400MHz,
CDCl3) |? ppm 8.29 (d, J = 7.80 Hz, 2H), 8.01 (t, J = 7.80, 7.80 Hz, 1H), 4.50 (q, J =
7.12, 7.12, 7.12 Hz, 2H), 1.47 (t, J = 7.13, 7.13 Hz, 3H). 13C-NMR (100 MHz, CDCl3)
|? ppm 164.6, 148.6, 138.2,127.8, 62.3,14.2,14.2. ESI MS: m/z = 224.1 [M+H]+
, 246.1
[M+Na]+
.
Diethyl 2,6-pyridinedicarboxylate Preparation Products And Raw materials
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Frapp's ChemicalNFTZ Co., Ltd. | +86 (576) 8169-6106 | sales@frappschem.com | China | 880 | 50 |
Capot Chemical Co.,Ltd. | +86-(0)57185586718 +86-13336195806 | sales@capot.com | China | 29791 | 60 |
Shanghai Time Chemicals CO., Ltd. | +86-021-57951555 +8617317452075 | jack.li@time-chemicals.com | China | 1803 | 55 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32957 | 60 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29884 | 58 |
Changzhou Ansciep Chemical Co., Ltd. | +86 519 86305871 | sales@ansciepchem.com | CHINA | 4241 | 58 |
Hubei Jusheng Technology Co.,Ltd. | 18871490254 | linda@hubeijusheng.com | CHINA | 28172 | 58 |
Changzhou Ditong Chemical Co.,Ltd | +86-0519-88299272 | info@edengenechem.com | China | 2158 | 58 |
Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | sales@chemdad.com | China | 39894 | 58 |
Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
View Lastest Price from Diethyl 2,6-pyridinedicarboxylate manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2021-10-29 | Diethyl 2,6-pyridinedicarboxylate
15658-60-3
|
US $1.10 / g | 1g | 99.00% | 100 Tons Min | Dideu Industries Group Limited | ||
2019-07-06 | Diethyl 2,6-pyridinedicarboxylate
15658-60-3
|
US $1.00 / KG | 1KG | 99% | Customized | Career Henan Chemical Co |
- Diethyl 2,6-pyridinedicarboxylate
15658-60-3
- US $1.10 / g
- 99.00%
- Dideu Industries Group Limited
- Diethyl 2,6-pyridinedicarboxylate
15658-60-3
- US $1.00 / KG
- 99%
- Career Henan Chemical Co
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