9-phenylanthracene
- CAS No.
- 602-55-1
- Chemical Name:
- 9-phenylanthracene
- Synonyms
- NSC 90796;9-phenylantracene;9-PHENYLANTHRACENE;Phenylanthracene,98%;anthracene,9-phenyl-;9-Phenylanthracene97%;9-Phenylanthracene>9-Phenylanthracene,98%;9-Phenylanthracene 97%;9-PHENYLANTHRACENE OEKANAL
- CBNumber:
- CB8778824
- Molecular Formula:
- C20H14
- Molecular Weight:
- 254.33
- MDL Number:
- MFCD00001252
- MOL File:
- 602-55-1.mol
- MSDS File:
- SDS
| Melting point | 153-155 °C (lit.) |
|---|---|
| Boiling point | 417 °C (lit.) |
| Density | 1.1180 (estimate) |
| refractive index | 1.7040 (estimate) |
| storage temp. | Sealed in dry,Room Temperature |
| solubility | Chloroform (Slightly), Ethyl Acetate (Slightly) |
| form | Solid |
| color | Off-white to pale brown |
| Sensitive | Light Sensitive |
| BRN | 1910570 |
| CAS DataBase Reference | 602-55-1(CAS DataBase Reference) |
| FDA UNII | DC63Z5S1UP |
| EPA Substance Registry System | Anthracene, 9-phenyl- (602-55-1) |
9-phenylanthracene price More Price(19)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | P18004 | 9-Phenylanthracene 98% | 602-55-1 | 5g | $183.6 | 2024-03-01 | Buy |
| Sigma-Aldrich | P18004 | 9-Phenylanthracene 98% | 602-55-1 | 1g | $86.3 | 2023-06-20 | Buy |
| TCI Chemical | P0138 | 9-Phenylanthracene >98.0%(GC) | 602-55-1 | 1g | $113 | 2024-03-01 | Buy |
| TCI Chemical | P0138 | 9-Phenylanthracene >98.0%(GC) | 602-55-1 | 5g | $394 | 2024-03-01 | Buy |
| Alfa Aesar | H64419 | 9-Phenylanthracene, 98% | 602-55-1 | 1g | $23.8 | 2021-12-16 | Buy |
9-phenylanthracene Chemical Properties,Uses,Production
Chemical Properties
Pale Yellow Plates
Uses
9-Phenylanthracene is used to synthesize organic light-emitting material intermediates.
Preparation
The synthesis of 9-phenylanthracene involved mixing phenylboronic acid (2.13 g, 17.49 mmol), 9-bromoanthracene (3 g, 11.66 mmol), Pd(PPh3)4 (140 mg, 0.12 mmol), K2CO3 (16 mL, 2 M), and ethanol (8 mL) in a 100 mL flask with anhydrous toluene (32 mL). The mixture was refluxed for 48 h under nitrogen. After cooled to room temperature, the reaction mixture was quenched with dilute hydrochloric acid solution and extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation. The crude product was further purified by silica gel column chromatography (CH2Cl2/petroleum ether (1:4,v/v)) to get a white powder (2.43 g, 81.9 %). 1H NMR (500 MHz, CDCl3) δ 8.53 (s, 1H), 8.08 (d, J = 8.5 Hz, 2H), 7.70 – 7.67 (m, 2H), 7.63 – 7.54 (m, 3H), 7.50 – 7.45 (m, 4H), 7.37 (ddd, J = 8.7, 6.5, 1.2 Hz, 2H). EI-MS (m/z): Calculated for C20H14: 254.33. Found [M+]: 253.02.
Synthesis of 9-phenylanthracene
Synthesis Reference(s)
Journal of the American Chemical Society, 79, p. 393, 1957 DOI: 10.1021/ja01559a042
Purification Methods
Chromatograph it on alumina in *C6H6 and recrystallise it from AcOH or toluene. [Beilstein 5 H 725, 5 II 639, 5 III 2462.]
9-phenylanthracene Preparation Products And Raw materials
Raw materials
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Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Hebei Xinsheng New Material Technology Co., LTD. | +86-16632316109 | xinshengkeji@xsmaterial.com | China | 1085 | 58 |
| Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 | info@spring-chem.com | China | 2068 | 57 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18775 | 58 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32957 | 60 |
| AB PharmaTech,LLC | 323-480-4688 | sales@acrospharmatech.com | United States | 989 | 55 |
| Beijing Green Guardee Technology Co., Ltd | 86-010-69706062 | sales2@greenguardee.com | CHINA | 650 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29881 | 58 |
| Xiamen AmoyChem Co., Ltd | +86-86-5926051114 +8618959220845 | sales@amoychem.com | China | 6383 | 58 |
| BAYNOE CHEM CO.,LTD | +86-21-34783353 +8615000719740 | baynoe@baynoe.com | CHINA | 934 | 58 |
| Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | sales@chemdad.com | China | 39894 | 58 |
View Lastest Price from 9-phenylanthracene manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2024-11-27 | 9-phenylanthracene
602-55-1
|
US $0.00 / KG | 1KG | 98%min | 30tons/month | WUHAN FORTUNA CHEMICAL CO., LTD | |
 |
2024-11-18 | 9-Phenylanthracene
602-55-1
|
US $0.00-0.00 / KG | 1KG | 98% | 1000KG | Shaanxi Dideu New Materials Co. Ltd | |
 |
2024-11-05 | 9-PHENYLANTHRACENE
602-55-1
|
US $0.00 / KG | 1KG | 98.00% | 150KG /month | Shanghai Daken Advanced Materials Co.,Ltd |
-
- 9-phenylanthracene
602-55-1
- US $0.00 / KG
- 98%min
- WUHAN FORTUNA CHEMICAL CO., LTD
-
- 9-Phenylanthracene
602-55-1
- US $0.00-0.00 / KG
- 98%
- Shaanxi Dideu New Materials Co. Ltd
-
- 9-PHENYLANTHRACENE
602-55-1
- US $0.00 / KG
- 98.00%
- Shanghai Daken Advanced Materials Co.,Ltd
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