1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
- CAS No.
- 95464-05-4
- Chemical Name:
- 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
- Synonyms
- Pd(dppf)2Cl2;Pd(dppf)Cl2.CH2Cl2;PdCl2(dppf)DCM;[PdCl2(dppf)]CH2Cl2;Palladium[PdCl2(dppf)]CH2Cl2;[1,1-Bis(diphenylphosphino)ferrocene]dichloropalladium(II) complex with dichloromethane PdCl2(dppf)CH2Cl2;CHEMDOSE;ex with dichL;adium(II),compL;Pd(dppf)Cl2 DCM
- CBNumber:
- CB1347621
- Molecular Formula:
- C34H28Cl2FeP2Pd.CH2Cl2
- Molecular Weight:
- 816.63
- MOL File:
- 95464-05-4.mol
- MSDS File:
- SDS
- Modify Date:
- 2024/8/11 15:28:25
Melting point | 275-280 °C(lit.) |
---|---|
Density | 1 g/cm3 |
storage temp. | Keep in dark place,Inert atmosphere,Room temperature |
solubility | Chloroform (Slightly), Methanol (Slightly) |
form | Powder |
color | orange-red |
Water Solubility | Insoluble in water. |
Stability | Light Sensitive |
CAS DataBase Reference | 95464-05-4(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
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Signal word | Warning | |||||||||
Hazard statements | H302+H312+H332-H315-H319-H335 | |||||||||
Precautionary statements | P261-P280-P301+P312-P302+P352+P312-P304+P340+P312-P305+P351+P338 | |||||||||
Hazard Codes | Xn | |||||||||
Risk Statements | 20/21/22-36/37/38-40-67-48/20/22 | |||||||||
Safety Statements | 23-24/25-26-36/37 | |||||||||
WGK Germany | 3 | |||||||||
TSCA | No | |||||||||
HS Code | 28439000 | |||||||||
NFPA 704 |
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1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex price More Price(10)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich(India) | 379670 | [1,1′-Bis(diphenylphosphino)ferrocene]dichloropalladium(II), complex with dichloromethane | 95464-05-4 | 1G | ₹4220 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | 379670 | [1,1′-Bis(diphenylphosphino)ferrocene]dichloropalladium(II), complex with dichloromethane | 95464-05-4 | 5G | ₹16061.7 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | 379670 | [1,1′-Bis(diphenylphosphino)ferrocene]dichloropalladium(II), complex with dichloromethane | 95464-05-4 | 25G | ₹70485 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | 379670 | [1,1′-Bis(diphenylphosphino)ferrocene]dichloropalladium(II), complex with dichloromethane | 95464-05-4 | 250G | ₹296358.9 | 2022-06-14 | Buy |
TCI Chemicals (India) | B2064 | [1,1'-Bis(diphenylphosphino)ferrocene]palladium(II) Dichloride Dichloromethane Adduct | 95464-05-4 | 1G | ₹5500 | 2022-05-26 | Buy |
1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex Chemical Properties,Uses,Production
Chemical Properties
orange/red solid
Uses
suzuki reaction
Application
1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex is an organometallic compound that can be used as a noble metal catalyst for carbonylation reactions, cross-coupling reactions, Suzuki reaction.
Synthesis
1. Dissolve 2.00 grams of sodium palladium chloride in 30mL of anhydrous ethanol to obtain the ethanol solution of sodium palladium chloride;
2. Dissolve 4.15 grams of 1,1 '-bis (diphenylphosphine) ferrocene in 41mL dichloromethane to obtain 1,1' -bis (diphenylphosphine) ferrocene dichloromethane solution;
3. Under stirring conditions, add the ethanol solution of sodium palladite chloride in step 1 to dichloromethane solution of 1, 1 '-bis (diphenylphosphine) ferrocene in step 2. Stir and react for 1h at 25℃. 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex crystal, yield 90.46%.
In this method, the target product 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex was synthesized directly with dichloromethane as the solvent in one step, eliminating the synthesis process of precursor PDCl2 (DPPF). The reaction process is simple, the synthesis cycle is short, easy to operate, and the purity of the synthesized product is 99.4%.
1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | Inquiry |
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DAVY CHEM LABS | +91-9603460845 +91-9493444489 | Hyderabad, India | 109 | 58 | Inquiry |
JIVICHEM SYNTHESIS PVT LTD | +91-7028392790 +91-7028392790 | Maharashtra, India | 337 | 58 | Inquiry |
INDIAN PLATINUM PRIVATE LIMITED | +91-9322395199 +91-9322395199 | Mumbai, India | 54 | 58 | Inquiry |
Evans Fine Chem | +91-9821340302 +91-9821340302 | Maharashtra, India | 286 | 58 | Inquiry |
Johnson Matthey Chemicals India Pvt Ltd | +91-9820622275 +91-9711869003 | Maharashtra, India | 69 | 58 | Inquiry |
Vineeth Precious Catalysts Pvt Ltd | +91-9049600004 +91-9049600004 | Mumbai, India | 29 | 58 | Inquiry |
Dhara Industries | +91-9322395199 +91-9322395199 | Mumbai, India | 190 | 58 | Inquiry |
CLEARSYNTH LABS LTD. | +91-22-45045900 | Hyderabad, India | 6351 | 58 | Inquiry |
A.J Chemicals | 91-9810153283 | New Delhi, India | 6124 | 58 | Inquiry |
Otto Chemie Pvt. Ltd. | +91 9820041841 | Mumbai, India | 5873 | 58 | Inquiry |
Supplier | Advantage |
---|---|
DAVY CHEM LABS | 58 |
JIVICHEM SYNTHESIS PVT LTD | 58 |
INDIAN PLATINUM PRIVATE LIMITED | 58 |
Evans Fine Chem | 58 |
Johnson Matthey Chemicals India Pvt Ltd | 58 |
Vineeth Precious Catalysts Pvt Ltd | 58 |
Dhara Industries | 58 |
CLEARSYNTH LABS LTD. | 58 |
A.J Chemicals | 58 |
Otto Chemie Pvt. Ltd. | 58 |
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