2-Isocyanatoethyl Acrylate
- CAS No.
- 13641-96-8
- Chemical Name:
- 2-Isocyanatoethyl Acrylate
- Synonyms
- AOI-VM;2-IsocyatoethylAcrylate;2-IsocyanatoethylAcrylate;2-isocyanatoethyl prop-2-enoate;2-(Acryloyloxy)ethyl Isocyanate;Acrylic Acid 2-Isocyanatoethyl Ester;2-Propenoic acid 2-isocyanatoethyl ester;2-IsocyanatoethylAcrylate ISO 9001：2015 REACH;2-IsocyanatoethylAcrylate(stabilizedwithBHT)>2-Isocyanatoethyl Acrylate (stabilized with BHT)
- CBNumber:
- CB51449627
- Molecular Formula:
- C6H7NO3
- Molecular Weight:
- 141.12
- MOL File:
- 13641-96-8.mol
- MSDS File:
- SDS
- Modify Date:
- 2024/7/22 19:45:42
| Melting point | -25 °C |
|---|---|
| Boiling point | 80-95 °C(Press: 15 Torr) |
| Density | 1.05 |
| vapor pressure | 21.4Pa at 20℃ |
| refractive index | 1.4470 to 1.4510 |
| Flash point | 97°C(lit.) |
| storage temp. | Keep in dark place,Inert atmosphere,2-8C |
| form | clear liquid |
| color | Colorless to Almost colorless |
| Specific Gravity | 1.10 |
| EPA Substance Registry System | 2-Propenoic acid, 2-isocyanatoethyl ester (13641-96-8) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS06 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Danger | |||||||||
| Hazard statements | H319-H330-H315-H335-H312-H301 | |||||||||
| Precautionary statements | P260-P271-P284-P304+P340-P310-P320-P403+P233-P405-P501-P264-P270-P301+P310-P321-P330-P405-P501-P264-P280-P302+P352-P321-P332+P313-P362-P280-P302+P352-P312-P322-P363-P501-P264-P280-P305+P351+P338-P337+P313P | |||||||||
| RIDADR | UN 2206 6.1/PG III | |||||||||
| HazardClass | 6.1 | |||||||||
| PackingGroup | III | |||||||||
| HS Code | 2929100090 | |||||||||
| NFPA 704 |
|
2-Isocyanatoethyl Acrylate price More Price(2)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemicals (India) | I0918 | 2-Isocyanatoethyl Acrylate (stabilized with BHT) min. 98.0 % | 13641-96-8 | 5G | ₹6900 | 2022-05-26 | Buy |
| TCI Chemicals (India) | I0918 | 2-Isocyanatoethyl Acrylate (stabilized with BHT) min. 98.0 % | 13641-96-8 | 25G | ₹19800 | 2022-05-26 | Buy |
2-Isocyanatoethyl Acrylate Chemical Properties,Uses,Production
Uses
2-Isocyanatoethyl Acrylate is an important compound intermediate commonly used in chemical research and development as an API for organic synthesis.
Synthesis
2-Isocyanatoethyl Acrylate is prepared by the reaction of phosgene, ethanolamine and 2-chloropropionyl chloride. The steps are as follows:
In a 500 mL four-necked flask equipped with a stirrer, condenser, thermometer and inner tube, 250 mL of toluene and 25 g (0.41 mol) of 2-aminoethanol were added, heated to 90° C. and supplied with about 20 g of hydrogen chloride gas. Then 56 g (0.44 mol) of 3-chloropropionic acid chloride was added dropwise over 90 minutes and heated at 90° C. for 1 hour. Thereafter, 80 g (0.81 mol) of phosgene was supplied. Dissolved phosgene was then removed by nitrogen gas bubbling. Subsequently, 0.4 g of phenothiazine and 0.4 g of 2,6-bis-t-butylhydroxytoluene were added, and 50 g of triethylamine (0.49 mol) was supplied, and the mixture was heated and stirred at 50° C. for 6 hours. Thereafter, the mixture was cooled to room temperature, the formed hydrochloride salt was filtered, and toluene was distilled off. By the above process, Mixture 2 containing the main product of 2-acryloyloxyethyl isocyanate (AOI) 55 g (0.35 mol) (87% yield) and the by-product of 2-acryloyloxyethyl acrylate (2547 ppm by mass) was obtained.
2-Isocyanatoethyl Acrylate Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | Inquiry |
|---|---|---|---|---|---|
| A.J Chemicals | 91-9810153283 | New Delhi, India | 6124 | 58 | Inquiry |
| TCI Chemicals (India) Pvt. Ltd. | 1800 425 7889 | New Delhi, India | 6778 | 58 | Inquiry |
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 | China | 20308 | 58 | Inquiry |
| Xiamen Yunfan Biotech Co.,Ltd. | +8618050056030 | China | 27 | 58 | Inquiry |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | China | 16209 | 58 | Inquiry |
| Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | China | 21669 | 55 | Inquiry |
| Shanghai Time Chemicals CO., Ltd. | +86-021-57951555 +8617317452075 | China | 1807 | 55 | Inquiry |
| career henan chemical co | +86-0371-86658258 +8613203830695 | China | 29826 | 58 | Inquiry |
| Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 | China | 13102 | 58 | Inquiry |
| Hefei TNJ Chemical Industry Co.,Ltd. | 0551-65418671 | China | 34571 | 58 | Inquiry |
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