ChemicalBook > Product Catalog >Pharmaceutical intermediates >OLED material intermediate >1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one

1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one

1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one Structure
CAS No.
94576-68-8
Chemical Name:
1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one
Synonyms
PI 907T;APi-307;JADEADD 307;JADEWIN 307;JADEWIN 907 T;Photoinitiator 307;photo sensitizer 907T;Photo Initiator PI 908;PHOTO INITIATOR TRUELICHT 908;1-(biphenyl-4-yl)-2methyl-2-morpholinylpropan-1-one
CBNumber:
CB53123192
Molecular Formula:
C20H23NO2
Molecular Weight:
309.4
MOL File:
94576-68-8.mol
MSDS File:
SDS
Modify Date:
2024/4/23 16:18:34

1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one Properties

Melting point 121-123 °C(Solv: benzene (71-43-2); ligroine (8032-32-4))
Boiling point 455.3±35.0 °C(Predicted)
Density 1.106±0.06 g/cm3(Predicted)
pka 4.90±0.10(Predicted)
EPA Substance Registry System 1-Propanone, 1-[1,1'-biphenyl]-4-yl-2-methyl-2-(4-morpholinyl)- (94576-68-8)

1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one Chemical Properties,Uses,Production

Uses

1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.

Synthesis

Synthesis_94576-68-8
To a solution of 1- (biphenyl-4-yl) -2-methyl-2-chloropropane-1-one synthesized in Step 3) was added 62.2 g of morpholine and 114 g of a saturated sodium carbonate solution, The reaction was carried out. After the completion of the reaction, the aqueous phase was separated and the aqueous phase was separated. After the organic phase was washed with an equal volume of water, the solvent was recovered under reduced pressure to give 1_ (biphenyl-4-yl) -2-morpholinylpropan-1-one. The recovered solvent was allowed to be applied directly to the next batch. The crude product was recrystallized from absolute ethanol, filtered and dried to give a white powder Solid 182.5 grams, the yield of 91%, 99.4% purity, the filtrate can be applied to the next batch of crude crystal 1~2 times.

1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one Preparation Products And Raw materials

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1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-one 1-(biphenyl-4-yl)-2-methyl-2-morpholinopropan-1-actone 1-([1,1'-Biphenyl]-4-yl)-2-methyl-2-morpholinopropan-1-one PI 907T 1-(biphenyl-4-yl)-2methyl-2-morpholinylpropan-1-one Photoinitiator 307 photo sensitizer 907T JADEWIN 907 T 1-Propanone, 1-[1,1'-biphenyl]-4-yl-2-methyl-2-(4-morpholinyl)- PHOTO INITIATOR TRUELICHT 908 JADEADD 307 JADEWIN 307 1-biphenyl-4-yl-2-methyl-2-morpholin-4-yl-propan-1-one Photo Initiator PI 908 APi-307 94576-68-8