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ChemicalBook > Product Catalog >Organic Chemistry >Carboxylic acids and derivatives >3-bromo-5-methylbenzoic acid

3-bromo-5-methylbenzoic acid

3-bromo-5-methylbenzoic acid Structure
CAS No.
58530-13-5
Chemical Name:
3-bromo-5-methylbenzoic acid
Synonyms
5-broMo-3-Methylbenzoic acid;3-bromo-5-methylbenzoic acid;Benzoic acid, 3-bromo-5-methyl-
CBNumber:
CB61558780
Molecular Formula:
C8H7BrO2
Molecular Weight:
215.04
MOL File:
58530-13-5.mol
MSDS File:
SDS
Modify Date:
2024/4/22 18:05:02
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3-bromo-5-methylbenzoic acid Properties

Melting point 178-179.5℃
Boiling point 320.3±30.0 °C(Predicted)
Density 1.599±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. Sealed in dry,Room Temperature
form solid
pka 3.88±0.10(Predicted)
color Pale yellow
InChIKey NWOMVQDBDBUANF-UHFFFAOYSA-N

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P305+P351+P338
HS Code  2916310090

3-bromo-5-methylbenzoic acid Chemical Properties,Uses,Production

Chemical Properties

Off-white powder

Synthesis

1-bromo-3,5-dimethylbenzene (15 g, 81 mmol, 1.0 eq) in a mixture of pyridine (133 mL) and H2O (83 mL) was heated to 80°C. KMnO4 (25.6 g, 162 mmol, 2.0 eq) was added in portions over 45 min. After the addition was completed, heating was continued at 80°C for 1.5 h. The hot solution was then filtered, and the filtrate was acidified by addition of concentrated hydrochloric acid. The aqueous solution was extracted with EtOAc and the combined organic extracts washed with water and brine, dried (Na2SO4), filtered and evaporated in vacuo. The residue was purified by column chromatography (CH2Cl2 : MeOH, 80:1 to 40:1) to give 3-bromo-5-methylbenzoic acid. White solid, yield (5.2 g, 29 %). LC-MS: m/z 212.9, 215 [M+H]+. 1H NMR (400 MHz, MeOD) δ 7.91 (s, 1H), 7.79 (s, 1H), 7.57 (s, 1H), 2.38 (s, 3H).
synthesis of 3-bromo-5-methylbenzoic acid

3-bromo-5-methylbenzoic acid Preparation Products And Raw materials

Raw materials

7-BROMO-5-METHYL-1H-INDOLE-2,3-DIONE (3-broMo-5-Methylphenyl)Methanol 2-AMINO-3-BROMO-5-METHYLBENZOIC ACID 1-BroMo-3-broMoMethyl-5-Methyl-benzene 3-BROMO-5-METHYLBENZONITRILE
2-Amino-5-methylbenzoic acid 5-Bromo-m-xylene Nitric acid
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Preparation Products

3-(aminomethyl)-5-bromobenzonitrile 3-Bromo-5-cyanobenzyl bromide

3-bromo-5-methylbenzoic acid Suppliers

Global( 129)Suppliers
Supplier Tel Country ProdList Advantage Inquiry
A.J Chemicals 91-9810153283 New Delhi, India 6124 58 Inquiry
Changzhou Anxuan Chemical Co., Ltd +86-0519-89882563 +86-18961279162 China 4328 58 Inquiry
Hebei Mojin Biotechnology Co., Ltd +86 13288715578 +8613288715578 China 12447 58 Inquiry
Henan Bao Enluo International TradeCo.，LTD +86-17331933971 +86-17331933971 China 2503 58 Inquiry
Capot Chemical Co.,Ltd. 571-85586718 +8613336195806 China 29798 60 Inquiry
career henan chemical co +86-0371-86658258 +8613203830695 China 29888 58 Inquiry
Accela ChemBio Inc. +1-858-6993322 United States 19479 58 Inquiry
Hebei Guanlang Biotechnology Co., Ltd. +86-19930503282 China 8821 58 Inquiry
Chongqing Chemdad Co., Ltd +86-023-6139-8061 +86-86-13650506873 China 39916 58 Inquiry
CONIER CHEM AND PHARMA LIMITED +8618523575427 China 49392 58 Inquiry
Supplier Advantage
A.J Chemicals 58
Changzhou Anxuan Chemical Co., Ltd 58
Hebei Mojin Biotechnology Co., Ltd 58
Henan Bao Enluo International TradeCo.，LTD 58
Capot Chemical Co.,Ltd. 60
career henan chemical co 58
Accela ChemBio Inc. 58
Hebei Guanlang Biotechnology Co., Ltd. 58
Chongqing Chemdad Co., Ltd 58
CONIER CHEM AND PHARMA LIMITED 58

58530-13-5(3-bromo-5-methylbenzoic acid)Related Search:

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3-bromo-5-methylbenzoic acid 5-broMo-3-Methylbenzoic acid Benzoic acid, 3-bromo-5-methyl- 58530-13-5