4-アミノベンジルシアニド 化学特性,用途語,生産方法
外観
白色～褐色、結晶～粉末又は塊
溶解性
熱水に難溶。エタノール, アセトンに可溶。エタノール及びアセトンに溶け、水にほとんど溶けない。
用途
有機合成原料。
化学的特性
yellow to brown crystalline powder, crystals
Synthesis Reference(s)
Synthetic Communications, 22, p. 3189, 1992
DOI: 10.1080/00397919208021132
合成
P-Nitrophenylacetonitrile (10 g, 61.67 mmol) was dissolved in methanol (50 mL). Add 10 per cent Pd/C (1.0g), Replace the reaction system four times with H2, and Stir at room temperature overnight in an H2 environment (0.5 MPa).TLC analysis, the reaction was complete, and the reaction solution was filtered through celite. The filtrate was concentrated under reduced pressure to give 8.08g of 4-Aminophenylacetonitrile; the yield was 99.1 per cent.
4-アミノベンジルシアニド 上流と下流の製品情報
原材料
準備製品