3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム

3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム 化学構造式
6448-97-1
CAS番号.
6448-97-1
化学名:
3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム
别名:
リッサミンブルーBF;C.I.アシッドブルー18;メランチンブルーBF;3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム;3-({4-アミノ-3-[(ソジオオキシ)スルホニル]フェニル}アミノ)-7-[エチル({3-[(ソジオオキシ)スルホニル]フェニル}メチル)アミノ]-5-(4-スルホナトフェニル)-5λ5-フェナジン-5-イリウム
英語名:
2-[benzenesulfonyl-(4-nitrophenyl)amino]-N-(2,4-dimethylpentan-3-yl)ac etamide
英語别名:
Acid Blue 18;C.I.Acid Blue 18;Merantine Blue BF;Lissamine Blue BF;Acid blue 18 (C.I. 50230);C.I.Acid Blue 18:C.I.50230;2-[N-(benzenesulfonyl)-4-nitroanilino]-N-(2,4-dimethylpentan-3-yl)acetamide;2-[benzenesulfonyl-(4-nitrophenyl)amino]-N-(2,4-dimethylpentan-3-yl)ac etamide;3-[(4-Amino-3-sodiosulfophenyl)amino]-7-[N-ethyl-N-(3-sodiosulfobenzyl)amino]-5-(4-sulfonatophenyl)phenazin-5-ium
CBNumber:
CB91261102
化学式:
C21H27N3O5S
分子量:
0
MOL File:
6448-97-1.mol

3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム 物理性質

安全性情報

3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム 価格

メーカー 製品番号 製品説明 CAS番号 包装 価格 更新時間 購入

3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム 化学特性,用途語,生産方法

製造方法

the molecular than 2-Amino-5-(4-nitroanilino)benzenesulfonic acid, 3-(Ethyl(phenyl)amino)methyl)benzenesulfonic acid, 2-Aminobenzenesulfonic acid with heavy chromium acid potassium and sulfuric acid oxidation, then use 4-Aminobenzenesulfonic acid further oxidation, reduction with the iron powder.

合成

Neutral solutions containing the sodium salt of 61 kg of 4-nitro-4- aminodiphenylamine-2-sulfonic acid in 500 L ofwater and the sodium salt of 57 kg of N-ethyl- N-benzylanilinesulfonic acid in 300 L water are combined in a 5000 L wooden vat equipped with a propeller stirrer. After the solution has been diluted with 1400 L of ice water, a solution containing 75.5 kg of sodium dichromate and 37.2 kg of sulfuric acid monohydrate in 4000 L water is added at 5 ℃. After stirring the mixture for 15 min, a neutral solution containing the sodium salt of 30.5 kg of aniline-4-sulfonic acid in 290 L of water is added. The mixture is again stirred for 15 min, then heated to 40 ℃ and stirred for 15 min. After rapid heating of the mixture to 80 ℃ with live steam, 11 kg of sodium carbonate is added. The reaction mixture, cooled to 70 ℃, is transferred to a 6000 L reduction vessel equipped with a propeller stirrer, mixed with 50 kg of iron filings, and stirred for 45 – 60 min. The alkaline spot test must show a brown rather a reddish blue spot. The reaction mixture is allowed to settle, then filtered through a filter press. The process of settling and filtration is repeated and the press is then washed, first with 1000 and then with 2000 L of water. The filtrate is salted out with 800 – 850 kg of common salt and, after stirring overnight at 18 – 20 ℃, filtered under suction. After drying under vacuum, 180 – 190 kg of the dye is obtained, corresponding to 360 – 380 kg of commercial-type Acid Cyanine BF.

Properties and Applications

red light navy blue. Soluble in cold water, hot water, ethanol to blue. The strong sulfuric acid for green, diluted into blue to red light purple. In aqueous solution for the navy blue join sodium hydroxide, and precipitation.
Standard Light Fastness Soaping Persperation Fastness Oxygen bleaching Fastness to seawater
Fading Stain Fading Stain Fading Stain
ISO 3 3 5 4-5 2 5 3-4 2
AATCC 3 2-3 2-3 1-2 1 1 4 4

3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム 上流と下流の製品情報

原材料

準備製品


3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム 生産企業

Global( 1)Suppliers
名前 電話番号 電子メール 国籍 製品カタログ 優位度
Hubei Jusheng Technology Co.,Ltd.
18871490254
linda@hubeijusheng.com CHINA 28180 58

6448-97-1(3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム)キーワード:


  • 6448-97-1
  • 2-[benzenesulfonyl-(4-nitrophenyl)amino]-N-(2,4-dimethylpentan-3-yl)ac etamide
  • Acid blue 18 (C.I. 50230)
  • 3-[(4-Amino-3-sodiosulfophenyl)amino]-7-[N-ethyl-N-(3-sodiosulfobenzyl)amino]-5-(4-sulfonatophenyl)phenazin-5-ium
  • C.I.Acid Blue 18
  • Lissamine Blue BF
  • Merantine Blue BF
  • 2-[N-(benzenesulfonyl)-4-nitroanilino]-N-(2,4-dimethylpentan-3-yl)acetamide
  • Acid Blue 18
  • C.I.Acid Blue 18:C.I.50230
  • リッサミンブルーBF
  • C.I.アシッドブルー18
  • メランチンブルーBF
  • 3-[(4-アミノ-3-ソジオスルホフェニル)アミノ]-7-[N-エチル-N-(3-ソジオスルホベンジル)アミノ]-5-(4-スルホナトフェニル)フェナジン-5-イウム
  • 3-({4-アミノ-3-[(ソジオオキシ)スルホニル]フェニル}アミノ)-7-[エチル({3-[(ソジオオキシ)スルホニル]フェニル}メチル)アミノ]-5-(4-スルホナトフェニル)-5λ5-フェナジン-5-イリウム
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