1-(2-hydroxy-5-nitrophenyl)propan-1-one
1-(2-hydroxy-5-nitrophenyl)propan-1-one 物理性質
- 融点 :
- 93-94 °C
- 沸点 :
- 299.3±25.0 °C(Predicted)
- 比重(密度) :
- 1.321±0.06 g/cm3(Predicted)
- 貯蔵温度 :
- Inert atmosphere,Room Temperature
- 酸解離定数(Pka):
- 5.45±0.30(Predicted)
安全性情報
- リスクと安全性に関する声明
- 危険有害性情報のコード(GHS)
1-(2-hydroxy-5-nitrophenyl)propan-1-one 価格
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1-(2-hydroxy-5-nitrophenyl)propan-1-one 化学特性,用途語,生産方法
製造方法
Preparation by Friedel–Crafts acylation of p-nitrophe-nol with propionyl chloride in nitrobenzene in the presence of aluminium chloride (36%)
Also obtained by Fries rearrangement of p-nitrophenyl propionate (m.p. 63–64°) in nitrobenzene in the presence of aluminium chloride at 125° for 5 h (23%)
Preparation by reaction of boron trichloride with 2-methoxy-5-nitropropiophe-none in methylene chloride, first at ?78°, then at r.t. for 14 h (92%). Also obtained by nitration of o-hydroxypropiophenone (23%), in acetic acid with fuming nitric acid, first at 0°, then at 60°
Also obtained by alkaline hydrolysis of 3-methyl-6-nitrochromone (m.p. 147–148°) (85%).
1-(2-hydroxy-5-nitrophenyl)propan-1-one 上流と下流の製品情報
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1-(2-hydroxy-5-nitrophenyl)propan-1-one 生産企業
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- 1-(2-hydroxy-5-nitrophenyl)propan-1-one
- 1-Propanone, 1-(2-hydroxy-5-nitrophenyl)-