1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산

1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산
1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산 구조식 이미지
카스 번호:
3141-04-6
한글명:
1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산
동의어(한글):
1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산
상품명:
1-(2,4-Cyclopentadiene-1-ylidene)cyclohexane
동의어(영문):
Pentamethylenefulvene;5-Cyclohexylidene-1,3-cyclopentadiene;(2,4-Cyclopentadienylidene)cyclohexane;Cyclohexane, 2,4-cyclopentadien-1-ylidene-;(2,4-Cyclopentadiene-1-ylidene)cyclohexane;1-(2,4-Cyclopentadiene-1-ylidene)cyclohexane
CBNumber:
CB52271531
분자식:
C11H14
포뮬러 무게:
146.23
MOL 파일:
3141-04-6.mol

1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산 속성

안전

1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산 C화학적 특성, 용도, 생산

Purification Methods

Purify the fulvene by column chromatography and eluting with n-hexane [Abboud et al. J Am Chem Soc 109 1334 1987]. Cyclohexyl mercaptan (cyclohexane thiol) [1569 -69 -3] M 116.2, b 38-39o/12mm, 5 7o/23mm, 90o/100mm, 157o/763mm, d 4 0.949, n D 1.493, pKEst ~10.8. Possible impurities are the sulfide and the disulfide. Purify the thiol by conversion to the Na salt by dissolving in 10% aqueous NaOH, extract the sulfide and disulfide with Et2O, and then acidify the aqueous solution (with cooling and under N2) with HCl, extract with Et2O, dry over MgSO4, evaporate and distil it in a vacuum (b 41o/12mm). The sulfide has b 7 4o/0.2mm, n D 1.5162 and the disulfide has b 110-112o/0.2mm, n D 1.5557. The Hg-mercaptide has m 77-78o (needles from EtOH). [Naylor J Chem Soc 1532 1947, Beilstein 6 H 8, 6 I 6, 6 II 14, 6 III 46, 6 IV 72.]

1-(2,4-사이클로펜타디엔-1-일리덴)사이클로헥산 준비 용품 및 원자재

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