| 24887-75-0 Basic information More.. |
Product Name: | androstane | Synonyms: | 1H-Cyclopenta(A)phenanthrene, hexadecahydro-10,13-dimethyl-, (8S-(8alpha,9beta,10alpha,13alpha,14beta))-;Androstane (van) | CAS: | 24887-75-0 | MF: | C19H32 | MW: | 260.46 | EINECS: | | Mol File: | 24887-75-0.mol | ![24887-75-0](/CAS/GIF/24887-75-0.gif) |
Use
Purify 5-androstane by chromatography through Al2O3 (grade III) and elute with pet ether and recrystallise from MeOH (2x) and Me2CO/MeOH. It sublimes at 60o/high vacuum. Also dissolve it in pet ether, filter it through silica gel, evaporate and recrystallise it. [Steiger & Reichstein Helv Chim Acta 20 817 1937, Prelog et al. Helv Chim Acta 27 66 1944, IR, NMR: Halkes & Havinga Rec Trav Chim Pays-Bas 8 4 889 1965, Allinger et al. Tetrahedron 27 5073 1971, Beilstein 5 III 1110, 5 IV 1211.]
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24887-75-0
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