N-Methyl-N-(trimethylsilyl)acetamide
| | 7449-74-3 Basic information More.. |
| Product Name: | N-Methyl-N-(trimethylsilyl)acetamide | | Synonyms: | N-Methyl-N-TMS-acetamide;N-Methyl-N-trimethylsilyl-acetamide(MSA);MSA~N-Trimethylsilyl-N-methylacetamide;N-Methyl-N-trimethylsilyacetamideMSA(N-Trimethylsilyl-N-methylacetamide);N-Methyl-N-trimethylsilylacetamine;N-Methyl-N-(trimethylsilyl)acetamide,98%;N-Methyl-N-trimethylsilylacetamide [Trimethylsilylating Agent];[TriMethylsilylating Agent] | | CAS: | 7449-74-3 | | MF: | C6H15NOSi | | MW: | 145.27 | | EINECS: | 231-217-0 | | Mol File: | 7449-74-3.mol |  |
Use
N-Methyl-N-trimethylsilylacetamide [7449-74-3] M 145.3, b 48 -49o/11mm, 8 4o/13mm, 105-107o/35mm (solid at room temperature), d 4 0.90, n D 1.4379. A likely impurity is Et3N.HCl which can be detected by its odour. If it is completely soluble in *C6H6, then redistil; otherwise dissolve it in this solvent, filter and evaporate first in a vacuum at 12mm, then fractionate; all operations should be carried out in a dry N2 atmosphere. [Klebe et al. J Am Chem Soc 88 3390 1966, Ried & Suarez-Rivero Chem Ber 96 1473 1963, Beilstein 4 IV 4011.]
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7449-74-3
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