| | 597-71-7 Basic information More.. |
| Product Name: | PENTAERYTHRITOL TETRAACETATE | | Synonyms: | 1,3-Propanediol, 2,2-bis[(acetyloxy)methyl]-, diacetate;1,3-Propanediol,2,2-bis[(acetyloxy)methyl]-,diacetate;3-(Acetyloxy)-2,2-bis[(acetyloxy)methyl]propyl acetate;3-propanediol,2,2-bis((acetyloxy)methyl)-diacetate;PENTAERYTHRITOL TETRAACETATE 98+%;2,2-BIS[(ACETYLOXY)METHYL]-1,3-PROPANEDIOL;2,2-BIS[(ACETYLOXY)METHYL]-1,3-PROPANEDIOL DIACETATE;TETRAHYDROXYMETHYLMETHANE TETRAACETATE | | CAS: | 597-71-7 | | MF: | C13H20O8 | | MW: | 304.29 | | EINECS: | 209-907-8 | | Mol File: | 597-71-7.mol |  |
Use
Crystallise pentaerythritol tetraacetate from hot water, then leach it with cold water until the odour of acetic acid is no longer detectable. It also crystallises from 95% EtOH after dissolving in CHCl3, washing with saturated NaHCO3, then H2O, drying over anhydrous CaCl2 and evaporating. It has been prepared by acetolysis of the tetranitrate in 95% yield [Wolfrom et al. J Am Chem Soc 73 874 1951]. [Breusch & Oguzer Chem Ber 88 1511 1955, LeFèvre et.al. J Chem Soc 16 1958, Beilstein 1 IV 1812, 2 IV 264.]
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597-71-7
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