(4'-METHYLBIPHENYL-3-YL)-METHANOL

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Products Intro: Product Name:(4'-Methyl-[1,1'-biphenyl]-3-yl)methanol
CAS:89951-79-1
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Products Intro: Product Name:(4'-Methyl-[1,1'-biphenyl]-3-yl)methanol
CAS:89951-79-1
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Products Intro: Product Name:(4'-METHYLBIPHENYL-3-YL)-METHANOL
CAS:89951-79-1
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Products Intro: Product Name:(4'-METHYLBIPHENYL-3-YL)-METHANOL
CAS:89951-79-1
Package:1g;5g;25g
(4'-METHYLBIPHENYL-3-YL)-METHANOL Basic information
Synthesis
Product Name:(4'-METHYLBIPHENYL-3-YL)-METHANOL
Synonyms:(4'-METHYLBIPHENYL-3-YL)-METHANOL;(4'-METHYL[1,1'-BIPHENYL]-3-YL)METHANOL;AKOS BAR-1215;RARECHEM AL BD 1348;3-(4-Tolyl)benzyl alcohol;4'-Methyl[1,1'-biphenyl]-3-methanol;(4'-Methyl-[1,1'-biphenyl]-3-yl)methanol
CAS:89951-79-1
MF:C14H14O
MW:198.26
EINECS:
Product Categories:pharmacetical
Mol File:89951-79-1.mol
(4'-METHYLBIPHENYL-3-YL)-METHANOL Structure
(4'-METHYLBIPHENYL-3-YL)-METHANOL Chemical Properties
Boiling point 346.3±11.0 °C(Predicted)
density 1.072±0.06 g/cm3(Predicted)
pka14.31±0.10(Predicted)
Safety Information
HS Code 2905190098
MSDS Information
(4'-METHYLBIPHENYL-3-YL)-METHANOL Usage And Synthesis
SynthesisTo a suspension of potassium flfluoride (350 mg, 6.0 mmol, spray dried) in DMF (50 mL) were added ethyldiflfluoro-(4-methyl)silane (560 mg, 3.0 mmol), 3-iodobenzyl alcohol (250 mg, 2.0 mmol), and (η3 -C3H5PdCl)2 (37 mg, 0.1 mmol). The resulting mixture was stirred at 100 °C for 15 h, cooled to room temperature, poured into saturated aqueous sodium bicarbonate solution, and extracted with diethyl ether (3 × 20 mL). The combined ethereal layer was then dried over magnesium sulfate. The solvent was removed under reduced pressure. The crude material was purifified by silica gel chromatography eluting a mixture of hexane:EtOAc (5:1) to give 340 mg (86%) of 3-hydroxymethyl-4´-methylbiphenyl as a colorless solid.Reference: Hatanaka, Y; Goda, K.; Okahara, Y.; Hiyama, T. Tetrahedron 1994, 50, 8301−8316.
(4'-METHYLBIPHENYL-3-YL)-METHANOL Preparation Products And Raw materials
Raw materialsTRI-P-TOLYLBISMUTHINE-->3-IODOBENZYL ALCOHOL-->3-(Hydroxymethyl)phenylboronic acid-->4-Bromotoluene
Tag:(4'-METHYLBIPHENYL-3-YL)-METHANOL(89951-79-1) Related Product Information
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