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| | Methanesulfenic acid chloride Basic information |
| Product Name: | Methanesulfenic acid chloride | | Synonyms: | Methanesulfenic acid chloride;Methanesulfenyl chloride;Methylsulfur monochloride;Methylthio chloride;Methanesulfenyl chloride (6CI,7CI,8CI,9CI) | | CAS: | 5813-48-9 | | MF: | CH3ClS | | MW: | 82.55 | | EINECS: | | | Product Categories: | | | Mol File: | 5813-48-9.mol |  |
| | Methanesulfenic acid chloride Chemical Properties |
| Boiling point | 27-28 °C(Press: 53-60 Torr) | | density | 1.172±0.06 g/cm3(Predicted) |
| | Methanesulfenic acid chloride Usage And Synthesis |
| Preparation | To a flask containing 23.6 gm (0.25 mole) of dimethyl disulfide at - 1 5 ° to -20°C is slowly added dropwise 34 gm (0.25 mole) of freshly distilled sulfuryl chloride while keeping the temperature at -15° to -20°C. The reaction mixture is stirred for 1 hr, and then distilled to afford 37.1 gm (90%), b.p. 27-28°C (53-60 mm Hg); NMR, 2.91 ppm (singlet). The crude product can also be used without distillation since most of the material is product.
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| | Methanesulfenic acid chloride Preparation Products And Raw materials |
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