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2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester

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2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Suppliers list
Company Name: Univar Solutions(China) Co., Ltd.
Tel: +8615902132654
Email: ivy.zhuang@univarsolutions.com
Products Intro: CAS:1882074-17-0
Package:1KG,100KG,1MT,100MT
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Basic information
Product Name:2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester
Synonyms:2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester
CAS:1882074-17-0
MF:C21H20O5
MW:352.38
EINECS:
Product Categories:
Mol File:1882074-17-0.mol
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Structure
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Chemical Properties
Boiling point 483.9±44.0 °C(Predicted)
density 1.137±0.06 g/cm3(Predicted)
Safety Information
MSDS Information
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Usage And Synthesis
PreparationThe preparation of 2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester is as follows:1: Methacrylic acid (3.56 g, 41.5 mmol) and 4-(dimethylamino)pyridine (0.17 g, 1.4 mmol) is added to a suspension of 1b (3.0 g, 13.9 mmol) in 40 ml dichloromethane. The reaction mixture is treated dropwise at 0° C. with a solution of N-(3-dimethylaminopropyl)-N′-ethylcarbodiimide (6.44 g, 41.5 mmol) in dichloromethane (20 ml) and stirred for 20 h at room temperature. After removing solvent in vacuo, the oily residue is purified by silica gel chromatography with dichloromethane/ethyl acetate 20:1 as eluent. The obtained product is recrystallized from acetonitril to afford white crystals of 1 (2.1 g, mp. 105° C.).

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2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Preparation Products And Raw materials
Tag:2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester(1882074-17-0) Related Product Information
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