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Bide Pharmatech Ltd.
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Product Name:Methanesulfinyl chloride CAS:676-85-7 Purity:90% Package:100mg;250mg;1g;
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ATK CHEMICAL COMPANY LIMITED
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CAS:676-85-7 Purity:98% Package:1G,5G,100G,500g,1kg
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Company Name: |
Bide Pharmatech Ltd.
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400-6005915 |
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sales@picasso-e.com |
Products Intro: |
Product Name:Methanesulfinyl chloride CAS:676-85-7 Purity:90% Package:100mg;250mg;1g
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| Methanesulfinylchloride Basic information |
Product Name: | Methanesulfinylchloride | Synonyms: | Methanesulfinylchloride;methylsulphinyl chloride;Methanesulfinyl chloride (6CI,7CI,8CI,9CI);Methanesulfinic Chloride | CAS: | 676-85-7 | MF: | CH3ClOS | MW: | 98.55 | EINECS: | | Product Categories: | | Mol File: | 676-85-7.mol | ![Methanesulfinylchloride Structure](CAS/GIF/676-85-7.gif) |
| Methanesulfinylchloride Chemical Properties |
Boiling point | 55-59 °C(Press: 40 Torr) | density | 1.494±0.06 g/cm3(Predicted) |
| Methanesulfinylchloride Usage And Synthesis |
Synthesis Reference(s) | The Journal of Organic Chemistry, 33, p. 2104, 1968 DOI: 10.1021/jo01269a088 Synthetic Communications, 24, p. 1207, 1994 DOI: 10.1080/00397919408011719 | Synthesis | A mixture of 23.5 g (0.25 mol) of freshly distilled dimethyl disulfide and 51 g (0.5 mol) of acetic anhydride is chlorinated at -10 to 0℃. During the course of the reaction the color changes from yellow to red and then disappears, at which point the addition of chlorine is suspended, leading to 126 g of reaction mixture. This is distilled in a 45 cm Vigreux column at 2 kPa with cooling. Acetyl chloride distills at 0℃, and at 47–48℃ the almost colorless methanesulfinyl chloride is obtained in 83–86% yield. |
| Methanesulfinylchloride Preparation Products And Raw materials |
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