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Product Name:Acetaldehyde 3-Bromopropyl Ethyl Acetal
CAS:34399-67-2
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| | 1-bromo-3-(1-ethoxyethoxy)propane Basic information |
| Product Name: | 1-bromo-3-(1-ethoxyethoxy)propane | | Synonyms: | 1-bromo-3-(1-ethoxyethoxy)propane;1-(1-Ethoxyethoxy)-3-bromopropane;3-broMo-n-propyl-1-ethoxyethyl ether;Acetaldehyde 3-Bromopropyl Ethyl Acetal;Propane, 1-bromo-3-(1-ethoxyethoxy)- | | CAS: | 34399-67-2 | | MF: | C7H15BrO2 | | MW: | 211.1 | | EINECS: | 251-997-6 | | Product Categories: | | | Mol File: | 34399-67-2.mol |  |
| | 1-bromo-3-(1-ethoxyethoxy)propane Chemical Properties |
| Boiling point | 184.4±15.0 °C(Predicted) | | density | 1.239±0.06 g/cm3(Predicted) | | solubility | sol common organic solvents (i.e. diethyl ether, THF, 1,3-propanediol) | | form | colorless liquid, bp 49-51 °C/1 mmHg | | EPA Substance Registry System | Propane, 1-bromo-3-(1-ethoxyethoxy)- (34399-67-2) |
| | 1-bromo-3-(1-ethoxyethoxy)propane Usage And Synthesis |
| Preparation | 1-Bromo-3-(1-ethoxyethoxy)propane has been prepared from 3-bromo-1-propanol and Ethyl Vinyl Ether using dichloroacetic acid as the catalyst.1 The choice of the catalyst was reported to be crucial to the success of the procedure. This preparation provided the product in 92% yield. | | storage | Storage, and Precautions: the reagent is acid sensitive and is stored at -30 °C over powdered sodium carbonate. This is an alkylation reagent; proper protective equipment should be worn and use restricted to a fume hood. | | Purification Methods | 1-Bromo-3-(1-ethoxyethoxy)propane is purified by vacuum distillation, boiling point 49-51°C/1 mmHg. | | References | 1. Eaton, P. E.; Cooper, G. F.; Johnson, R. C.; Mueller, R. H. JOC 1972, 37, 1947. |
| | 1-bromo-3-(1-ethoxyethoxy)propane Preparation Products And Raw materials |
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