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Postion:Product Catalog >Organic Chemistry>Ketones>2-(2-chlorophenyl)cyclohexanone
2-(2-chlorophenyl)cyclohexanone
  • 2-(2-chlorophenyl)cyclohexanone
  • 2-(2-chlorophenyl)cyclohexanone
  • 2-(2-chlorophenyl)cyclohexanone
  • 2-(2-chlorophenyl)cyclohexanone
  • 2-(2-chlorophenyl)cyclohexanone

2-(2-chlorophenyl)cyclohexanone NEW

Price Get Latest Price
Package 1KG 5KG 25KG
Min. Order: 1KG
Supply Ability: 20 T each week
Update Time: 2023-08-11

Product Details

Product Name: 2-(2-chlorophenyl)cyclohexanone CAS No.: 91393-49-6
EC-No.: 679-869-9 Min. Order: 1KG
Purity: 98%~99% Supply Ability: 20 T each week
Release date: 2023/08/11

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2-(2-chlorophenyl)cyclohexanone Basic information
Product Name:2-(2-chlorophenyl)cyclohexanone
Synonyms:2-(2-chlorophenyl)cyclohexanone;2-(2-chlorophenyl)cyclohexan-1-one;Cyclohexanone, 2-(2-chlorophenyl)-;(2-chlorophenyl)cyclohexanone;2-(2-Chlor-phenyl)-cyclohexanon
CAS:91393-49-6
MF:C12H13ClO
MW:208.68
EINECS:679-869-9
Product Categories:intermediates;91393-49-6;Pharm
Mol File:91393-49-6.mol
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2-(2-chlorophenyl)cyclohexanone Chemical Properties
Melting point 60-62 °C
Boiling point 308.8±42.0 °C(Predicted)
density 1.165±0.06 g/cm3(Predicted)
form powder
color white crystalline
InChIInChI=1S/C12H13ClO/c13-11-7-3-1-5-9(11)10-6-2-4-8-12(10)14/h1,3,5,7,10H,2,4,6,8H2
InChIKeyUOEXWLLNMGAJDD-UHFFFAOYSA-N
SMILESC1(=O)CCCCC1C1=CC=CC=C1Cl
Chemical Propertieswhite crystalline powder.
Uses2-(2-Chlorophenyl)-cyclohexanone is a reactant that is used in the preparation of benzofurans via palladium-phosphine-catalyzed intramolecular enolate O-arylation of α-arylketones.
SynthesisTo a flame dried flask was added Cs2CO3 (6.5 g, 20 mmol), Pd2(dba)3 (184 mg, 0.2 mmol) and Xantphos (139 mmol, 0.24 mmol). After purging with N2, toluene (10 mL), ketone (15 mmol) and phenyl iodide (1.11 mL, 10 mmol) were added. After stirring overnight at 80 .MALE.C, the mixture was filtered and concentrated in vacuo to afford a residue, which was purified by flash chromatography to provide the desired 2-(2-chlorophenyl)cyclohexanone.





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