4,4'-Trimethylenebis(1-methylpiperidine)(64168-11-2) Raman
Product Name4,4'-Trimethylenebis(1-methylpiperidine)
CAS64168-11-2
Molecular FormulaC15H30N2
Molecular Weight238.41
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MassMS-IW-1270 4,4'-trimethylenebis(1-methylpiperidine) C15H30N2 (Mass of molecular ion: 238)
Source Temperature: 230 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 1.0 29.0 2.6 30.0 1.2 39.0 1.4 41.0 5.9 42.0 15.5 43.0 13.0 44.0 30.0 53.0 1.4 55.0 9.8 56.0 2.4 57.0 7.3 58.0 27.2 59.0 1.5 67.0 2.0 68.0 1.3 69.0 1.6 70.0 34.8 71.0 10.4 72.0 3.6 79.0 1.0 81.0 2.0 82.0 2.4 83.0 1.3 84.0 2.1 94.0 2.1 96.0 52.2 97.0 5.5 98.0 24.0 99.0 14.0 100.0 1.0 110.0 4.1 112.0 21.0 113.0 5.0 118.0 4.1 122.0 1.3 124.0 1.3 126.0 20.7 127.0 6.2 138.0 2.2 140.0 32.0 141.0 4.3 152.0 1.1 154.0 1.4 166.0 4.6 167.0 1.5 168.0 13.3 169.0 1.8 178.0 1.3 180.0 3.8 181.0 5.9 182.0 4.6 192.0 2.2 194.0 11.2 195.0 7.0 196.0 1.5 207.0 1.3 208.0 5.2 209.0 6.0 210.0 2.5 221.0 1.0 223.0 100.0 224.0 16.1 225.0 1.2 236.0 1.9 237.0 34.7 238.0 59.0 239.0 10.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H30 N2 0.05 ml : 0.5 ml CDCl3 4,4'-trimethylenebis(1-methylpiperidine) 
Assign. Shift(ppm)
A 2.825 B 2.251 C 1.882 D 1.661 E 1.28 F 1.22 to 1.20
Hz ppm Int.1135.50 2.842 130 1123.66 2.812 136 899.54 2.251 1000 763.31 1.910 89 751.95 1.882 154 740.48 1.853 82 669.80 1.676 90 667.60 1.671 95 657.23 1.645 130 520.02 1.302 42 512.94 1.284 61 511.11 1.279 58 502.44 1.258 72 498.78 1.249 78 490.48 1.228 142 486.08 1.217 198 478.76 1.198 256 471.44 1.180 90
in CDCl3
liquid film
