4-硝基苯肼(100-16-3)核磁图(1HNMR)
InChI:InChI=1S/C6H7N3O2/c7-8-5-1-3-6(4-2-5)9(10)11/h1-4,8H,7H2
InChIKey: KMVPXBDOWDXXEN-UHFFFAOYSA-N
Smiles:N(C1=CC=C([N+]([O-])=O)C=C1)N
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Mass
MS-NW-4719
(p-nitrophenyl)hydrazine
C6H7N3O2 (Mass of molecular ion: 153)
Source Temperature: 170 °C
Sample Temperature: 120 °C
Direct, 75 eV
18.0 3.2
27.0 1.8
28.0 5.2
29.0 2.5
30.0 6.0
31.0 2.8
37.0 1.9
38.0 4.4
39.0 10.0
40.0 1.5
41.0 3.9
43.0 1.0
50.0 8.8
51.0 9.7
52.0 9.3
53.0 10.9
54.0 2.7
61.0 1.4
62.0 3.2
63.0 22.7
64.0 13.7
65.0 7.3
66.0 1.6
67.0 1.8
74.0 3.0
75.0 3.1
76.0 5.3
77.0 8.8
78.0 4.9
79.0 3.9
80.0 20.2
81.0 1.7
90.0 32.1
91.0 12.5
92.0 3.2
93.0 1.4
105.0 2.4
106.0 5.4
107.0 16.5
108.0 2.1
122.0 1.4
123.0 18.4
124.0 1.5
137.0 1.5
138.0 1.6
151.0 1.4
153.0 100.0
154.0 7.7
400 MHz in DMSO-d6
90 MHz in DMSO-d6
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| 1H NMR |
399.65 MHz |
| C6 H7 N3 O2
|
0.041 g : 0.5 ml DMSO-d6
|
| (p-nitrophenyl)hydrazine
|
 |
Assign. Shift(ppm)
A 8.41
B 8.011
C 6.815
D 4.51
|
Hz ppm Int.
3360.47 8.409 458
3352.78 8.390 29
3206.54 8.024 802
3197.14 8.000 842
2736.21 6.847 25
2728.03 6.827 449
2719.12 6.804 440
2710.08 6.782 28
2709.23 6.780 24
1812.74 4.536 25
1811.89 4.534 25
1802.37 4.510 1000
1793.21 4.487 43
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| 1H NMR |
89.56 MHz |
| C6 H7 N3 O2
|
0.044 g : 0.5 ml DMSO-d6
|
| (p-nitrophenyl)hydrazine
|
|
Assign. Shift(ppm)
A 8.35
B 8.00
C 6.81
D 4.48
|
Hz ppm Int.
747.88 8.351 227
724.38 8.089 68
721.25 8.054 741
719.25 8.031 201
717.31 8.010 45
716.25 7.998 29
713.94 7.972 204
711.94 7.950 913
708.81 7.915 99
617.38 6.894 107
614.25 6.859 1000
612.13 6.835 254
609.63 6.807 30
608.69 6.797 22
606.94 6.777 217
604.88 6.754 821
601.75 6.719 92
400.75 4.475 596