1193-12-0

3,3-二甲基哌啶(1193-12-0)核磁图(¹HNMR)

产品名称:3,3-二甲基哌啶

CAS:1193-12-0

分子式:C7H15N

分子量: 113.2

InChI:InChI=1S/C7H15N/c1-7(2)4-3-5-8-6-7/h8H,3-6H2,1-2H3

InChIKey: CDODDZJCEADUQQ-UHFFFAOYSA-N

Smiles:N1CCCC(C)(C)C1

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-3512          
3,3-dimethylpiperidine
C7H15N              (Mass of molecular ion:    113)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       1.0
      27.0       6.2
      28.0       9.8
      29.0      10.6
      30.0      24.9
      39.0       9.8
      40.0       1.9
      41.0      20.5
      42.0      10.5
      43.0      12.1
      44.0     100.0
      45.0       4.3
      53.0       2.9
      54.0       1.9
      55.0      11.6
      56.0      31.5
      57.0      51.7
      58.0       2.6
      67.0       3.3
      68.0       2.7
      69.0       3.7
      70.0      15.5
      71.0       3.0
      80.0       1.0
      81.0       1.3
      82.0       2.9
      83.0       2.0
      84.0       4.9
      85.0       1.6
      96.0       2.4
      97.0       1.0
      98.0      17.3
      99.0       1.2
     112.0      10.0
     113.0      37.1
     114.0       3.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₅ N	0.05 ml : 0.5 ml CDCl₃
3,3-dimethylpiperidine

    Assign.     Shift(ppm)

      A             2.720
      B             2.468
      C             2.28
      D             1.489
      E             1.336
      F             0.906

     Hz     ppm     Int.

   1092.53   2.734     82
   1087.16   2.721    108
   1081.54   2.707     86
    986.33   2.468    321
    912.48   2.284     71
    607.42   1.520     31
    601.32   1.505     64
    595.58   1.491     99
    590.21   1.477     76
    584.23   1.462     47
    539.55   1.351    111
    533.33   1.335    115
    527.34   1.320     77
    363.16   0.909    645
    362.30   0.907   1000
    350.71   0.878     28

in CDCl3