1497-17-2

2-甲基-2-苯基琥珀酰亚胺(1497-17-2)Raman光谱

产品名称:2-甲基-2-苯基琥珀酰亚胺

CAS:1497-17-2

分子式:C11H11NO2

分子量: 189.21

Mass

MS-NW-7963          
2-methyl-2-phenylsuccinimide
C11H11NO2           (Mass of molecular ion:    189)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      27.0       1.5
      39.0       5.3
      41.0       1.1
      50.0       3.3
      51.0       8.4
      52.0       1.9
      57.0       1.1
      57.5       3.4
      58.0       9.1
      58.5       1.0
      59.0       1.1
      63.0       2.7
      65.0       2.3
      70.0       1.0
      73.0       1.2
      74.0       1.3
      75.0       1.2
      76.0       1.6
      77.0      10.6
      78.0      11.2
      89.0       1.3
      91.0       6.8
     102.0       2.5
     103.0      16.0
     104.0       1.7
     115.0       5.7
     116.0       1.7
     117.0      29.3
     118.0     100.0
     119.0      10.4
     189.0      24.6
     190.0       3.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₁ H₁₁ N O₂	0.042 g : 0.5 ml CDCl₃
2-methyl-2-phenylsuccinimide

    Assign.     Shift(ppm)

      A             9.2
      B          7.37 to 7.33
      C     *1      3.107
      D     *1      2.904
      E             1.729
     
     J(C,D)=-18.4HZ

     Hz     ppm     Int.

    824.63   9.208     33
    667.81   7.457     25
    666.31   7.440     44
    664.63   7.422    105
    663.75   7.412     78
    661.19   7.383    247
    658.44   7.352    879
    655.44   7.319    202
    653.00   7.292    109
    651.31   7.273     82
    647.44   7.230     40
    646.94   7.224     38
    292.94   3.271     85
    274.56   3.066    330
    263.94   2.948    365
    245.56   2.742     95
    160.50   1.793     35
    154.94   1.731   1000
    149.88   1.674     29

in CDCl3