18156-15-5

(3-氰基丙基)二甲基氯硅烷(18156-15-5)质谱(MS)

产品名称:(3-氰基丙基)二甲基氯硅烷

CAS:18156-15-5

分子式:C6H12ClNSi

分子量: 161.7

InChI:InChI=1S/C6H12ClNSi/c1-9(2,7)6-4-3-5-8/h3-4,6H2,1-2H3

InChIKey: GPIARXZSVWTOMD-UHFFFAOYSA-N

Smiles:C(#N)CCC[Si](Cl)(C)C

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-7680          
chloro(3-cyanopropyl)dimethylsilane
C6H12ClNSi          (Mass of molecular ion:    161)

   Source Temperature: 270 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       1.8
      28.0       2.4
      29.0       1.5
      39.0       2.1
      41.0       1.9
      42.0       1.4
      43.0       5.9
      53.0       1.0
      55.0       1.0
      58.0       1.0
      59.0       1.4
      63.0      12.9
      64.0       1.4
      65.0      10.7
      67.0       2.9
      77.0       1.8
      78.0       2.6
      79.0       4.5
      80.0       1.1
      81.0       1.5
      84.0       1.2
      85.0       1.3
      90.0       1.7
      92.0       2.0
      93.0     100.0
      94.0       7.8
      95.0      35.5
      96.0       2.5
      97.0       1.4
      98.0      13.7
      99.0       1.5
     104.0       2.0
     105.0       1.0
     118.0      32.0
     119.0       3.6
     120.0      12.1
     121.0       1.3
     126.0       3.2
     133.0      37.7
     134.0       3.9
     135.0      13.3
     136.0       1.4
     146.0       8.0
     148.0       2.9
     167.0       1.1
     200.0       1.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₂ Cl N Si	0.05 ml : 0.5 ml CDCl₃
chloro(3-cyanopropyl)dimethylsilane

    Assign.     Shift(ppm)

      A             2.406
      B             1.79
      C             0.99
      D             0.445

     Hz     ppm     Int.

    224.13   2.503     43
    223.25   2.493     42
    216.81   2.421    125
    210.38   2.350     81
    159.94   1.786     34
    152.50   1.703     42
     95.81   1.070     80
     91.94   1.027     39
     87.75   0.980     44
     86.25   0.964     40
     84.19   0.941     34
     79.25   0.885     41
     78.63   0.878     38
     43.19   0.483     81
     39.94   0.446   1000
     36.44   0.407     44

in CDCl3