18402-83-0

3-壬烯-2-酮(18402-83-0)红外图谱(IR1)

产品名称:3-壬烯-2-酮

CAS:18402-83-0

分子式:C9H16O

分子量: 140.22

Mass

MS-IW-6977          
trans-3-nonen-2-one
C9H16O              (Mass of molecular ion:    140)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.3
      27.0       9.7
      28.0       2.2
      29.0      15.3
      39.0       9.3
      40.0       2.3
      41.0      21.4
      42.0       4.9
      43.0      63.8
      44.0       1.8
      51.0       1.1
      53.0       4.1
      54.0       1.9
      55.0     100.0
      56.0       4.8
      57.0       4.8
      58.0       2.0
      59.0       2.4
      67.0       6.8
      68.0       3.5
      69.0      14.2
      70.0       2.6
      71.0      24.5
      72.0       4.7
      79.0       2.7
      81.0       5.0
      82.0      17.3
      83.0       6.0
      84.0       5.9
      85.0       6.5
      93.0       1.6
      95.0       1.4
      96.0       1.2
      97.0      28.0
      98.0       4.0
      99.0       1.7
     107.0       1.1
     111.0       7.4
     112.0       1.0
     122.0       1.6
     125.0      47.8
     126.0       4.3
     140.0       5.3
     141.0       1.9

90 MHz in CDCl3

400 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₆ O	0.05 ml : 0.5 ml CDCl₃
trans-3-nonen-2-one

    Assign.     Shift(ppm)

      A             6.80
      B             6.080
      C             2.240
      D             2.20
      E             1.42
      F             1.31
      G             0.90

     Hz     ppm     Int.

    619.06   6.913     55
    612.31   6.837     33
    609.81   6.809     41
    603.13   6.735     84
    596.38   6.660     45
    552.00   6.164     57
    550.63   6.149     96
    549.25   6.133     49
    536.06   5.986     34
    534.69   5.971     60
    533.31   5.955     32
    200.69   2.241   1000
    196.94   2.199    100
    191.69   2.141     50
    189.81   2.120     44
    139.63   1.560     34
    137.00   1.530     34
    134.44   1.502     42
    131.63   1.470     60
    125.94   1.407     84
    122.81   1.372    172
    121.69   1.359    179
    120.56   1.347    167
    118.56   1.324    141
    117.00   1.307    122
    112.75   1.259     66
    111.50   1.245     58
    111.00   1.240     59
    109.50   1.223     48
    108.94   1.217     48
     86.00   0.961     78
     80.50   0.899    218
     74.38   0.831     54

¹H NMR	399.65 MHz
C₉ H₁₆ O	0.05 ml : 0.5 ml CDCl₃
trans-3-nonen-2-one

    Assign.     Shift(ppm)

      A             6.819
      B             6.075
      C             2.245
      D             2.23
      E             1.476
      F             1.32
      G             0.899

     Hz     ppm     Int.

   2740.60   6.858     38
   2733.64   6.841     79
   2726.81   6.823     41
   2724.61   6.818     44
   2717.77   6.801     87
   2710.82   6.783     43
   2437.26   6.099     56
   2435.79   6.095    104
   2434.20   6.091     56
   2421.26   6.059     50
   2419.80   6.055     96
   2418.21   6.051     50
    901.61   2.256     59
    900.15   2.253     80
    897.46   2.246   1000
    894.53   2.239    118
    893.19   2.235    117
    886.72   2.219     97
    885.38   2.216     91
    879.88   2.202     51
    878.42   2.198     49
    598.75   1.499     51
    595.95   1.492     30
    591.19   1.480     74
    588.50   1.473     37
    583.86   1.461     54
    535.52   1.340     49
    534.79   1.339     54
    532.84   1.334    115
    529.91   1.326    123
    528.93   1.324    146
    527.83   1.321     99
    525.39   1.315    162
    521.61   1.306    107
    518.07   1.297     48
    517.21   1.295     46
    366.46   0.917    120
    364.75   0.913     66
    362.79   0.908     67
    361.94   0.906     74
    360.84   0.903     90
    359.38   0.900    383
    355.59   0.890     56
    353.64   0.885     73
    352.29   0.882    122

in CDCl3