24016-03-3

2-氨基-3-苄氧基吡啶(24016-03-3)红外图谱(IR2)

产品名称:2-氨基-3-苄氧基吡啶

CAS:24016-03-3

分子式:C12H12N2O

分子量: 200.24

InChI:InChI=1S/C12H12N2O/c13-12-11(7-4-8-14-12)15-9-10-5-2-1-3-6-10/h1-8H,9H2,(H2,13,14)

InChIKey: NMCBWICNRJLKKM-UHFFFAOYSA-N

Smiles:C1(N)=NC=CC=C1OCC1=CC=CC=C1

Mass

MS-IW-0800          
3-benzyloxy-2-pyridinamine
C12H12N2O           (Mass of molecular ion:    200)

   Source Temperature: 110 °C
   Sample Temperature:  80 °C
   Direct, 75 eV

      39.0       2.7
      65.0       5.6
      81.0       2.9
      91.0     100.0
      92.0       8.0
     106.0       2.4
     109.0       4.9
     183.0       5.6
     184.0       1.3
     199.0       6.5
     200.0      50.2
     201.0       7.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₂ N₂ O	0.037 g : 0.5 ml CDCl₃
3-benzyloxy-2-pyridinamine

    Assign.     Shift(ppm)

      A             7.669
      B             7.40
      C             7.35
      D             6.941
      E             6.571
      F             5.043
      G             4.8

     Hz     ppm     Int.

   3068.24   7.678    197
   3066.89   7.674    206
   3063.23   7.665    212
   3061.89   7.662    208
   2966.55   7.423     41
   2964.11   7.417     82
   2961.55   7.411     57
   2957.89   7.402    732
   2956.05   7.397    438
   2952.03   7.387    374
   2951.29   7.385    471
   2949.10   7.380    113
   2947.39   7.375     50
   2945.68   7.371    106
   2944.34   7.368    135
   2943.48   7.366    147
   2941.04   7.360    119
   2938.72   7.354    142
   2935.91   7.347    108
   2933.35   7.340     93
   2932.25   7.338    112
   2928.10   7.327     44
   2926.39   7.323     37
   2925.78   7.321     33
   2779.05   6.954    167
   2777.71   6.951    169
   2771.24   6.935    190
   2769.90   6.931    188
   2632.57   6.588    226
   2627.56   6.575    226
   2624.88   6.568    210
   2619.75   6.556    208
   2015.50   5.044   1000
   1913.45   4.788    100

in CDCl3