43217-28-3

2-氯-9,10-二苯基蒽(43217-28-3)核磁图(¹HNMR)

产品名称:2-氯-9,10-二苯基蒽

CAS:43217-28-3

分子式:C26H17Cl

分子量: 364.87

Mass

MS-NW-7553          
2-chloro-9,10-diphenylanthracene
C26H17Cl            (Mass of molecular ion:    364)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

     136.0       1.0
     137.0       2.1
     138.0       1.1
     143.5       1.8
     149.0       3.0
     149.5       1.3
     150.0       4.7
     150.5       1.5
     151.0       2.1
     155.5       1.8
     156.0       1.3
     156.5       7.4
     157.0       3.8
     157.5       1.0
     161.0       1.9
     161.5       1.2
     162.0       5.9
     162.5       2.6
     163.0       9.9
     163.5       5.0
     164.0       4.7
     164.5       3.7
     182.0       1.6
     224.0       1.1
     248.0       1.4
     249.0       1.0
     250.0       5.6
     251.0       2.3
     252.0      11.7
     253.0       2.8
     274.0       1.5
     286.0       5.6
     287.0       4.5
     288.0       2.6
     289.0       2.0
     298.0       1.8
     299.0       1.0
     300.0       2.7
     301.0       1.4
     302.0       1.7
     313.0       3.6
     314.0       1.7
     322.0       1.4
     323.0       1.1
     324.0       5.9
     325.0       2.9
     326.0      17.8
     327.0      16.9
     328.0      17.5
     329.0      10.1
     330.0       3.4
     362.0       1.1
     363.0       3.5
     364.0     100.0
     365.0      29.7
     366.0      36.0
     367.0       9.2
     368.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₆ H₁₇ Cl	0.038 g : 0.5 ml CDCl₃
2-chloro-9,10-diphenylanthracene

    Assign.     Shift(ppm)

      A          7.67 to 7.66
      B             7.61
      C             7.58
      D             7.55
      E             7.438
      F             7.324
      G             7.217

     Hz     ppm     Int.

   3071.29   7.685    252
   3070.56   7.684    294
   3068.73   7.679    259
   3067.75   7.677    304
   3066.89   7.674    297
   3066.16   7.673    311
   3064.58   7.669    381
   3063.35   7.666    399
   3061.04   7.660    720
   3059.33   7.656    683
   3057.62   7.651    430
   3056.88   7.649    367
   3054.81   7.644    482
   3048.95   7.630    160
   3047.73   7.626    162
   3045.41   7.621    524
   3044.92   7.619    492
   3042.48   7.613    272
   3040.77   7.609    240
   3039.31   7.605    256
   3037.11   7.600    369
   3035.64   7.596    611
   3034.06   7.592    415
   3032.84   7.589    299
   3030.52   7.583    640
   3028.56   7.579    732
   3026.12   7.572    255
   3023.44   7.566    661
   3022.71   7.564    677
   3021.00   7.560    371
   3020.14   7.557    285
   3018.31   7.553    439
   3016.72   7.549    321
   3015.63   7.546    349
   3011.47   7.536    297
   3008.06   7.527    154
   2977.91   7.452    620
   2976.44   7.448   1000
   2974.85   7.444    682
   2972.53   7.438    291
   2971.44   7.436    372
   2969.97   7.432    695
   2968.51   7.428    755
   2967.04   7.425    374
   2931.27   7.335    428
   2930.79   7.334    407
   2928.83   7.329    287
   2926.88   7.324    318
   2925.17   7.320    304
   2923.22   7.315    271
   2921.14   7.310    400
   2889.89   7.232    360
   2887.70   7.226    343
   2880.49   7.208    343
   2878.42   7.203    321

in CDCl3