90-04-0

邻甲氧基苯胺(90-04-0)Raman光谱

产品名称:邻甲氧基苯胺

CAS:90-04-0

分子式:C7H9NO

分子量: 123.15

InChI:InChI=1S/C7H9NO/c1-9-7-5-3-2-4-6(7)8/h2-5H,8H2,1H3

InChIKey: VMPITZXILSNTON-UHFFFAOYSA-N

Smiles:C1(N)=CC=CC=C1OC

Mass

MS-NW-0463          
o-anisidine
C7H9NO              (Mass of molecular ion:    123)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.8
      18.0       2.2
      26.0       1.3
      27.0       4.5
      28.0       5.2
      37.0       1.3
      38.0       3.0
      39.0       8.5
      40.0       1.2
      41.0       3.0
      42.0       1.2
      43.0       1.0
      50.0       3.3
      51.0       6.2
      52.0      10.8
      53.0      15.2
      54.0       3.2
      62.0       1.4
      63.0       3.3
      64.0       1.8
      65.0      10.4
      66.0       2.2
      77.0       2.8
      78.0       2.6
      79.0       2.1
      80.0      65.8
      81.0       4.4
      91.0       1.5
      92.0       5.6
      93.0       2.1
      94.0       2.1
     105.0       2.7
     106.0       1.4
     108.0      98.1
     109.0       7.5
     122.0       1.2
     123.0     100.0
     124.0       8.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₉ N O	0.05 ml : 0.5 ml CDCl₃
o-anisidine

    Assign.     Shift(ppm)

      A             6.76
      B             6.74
      C             6.700
      D             6.653
      E             3.769
      F             3.7

     Hz     ppm     Int.

   2710.69   6.783     66
   2708.86   6.779     76
   2703.49   6.765    153
   2701.78   6.761    185
   2700.20   6.757     90
   2698.36   6.752    115
   2696.41   6.747     97
   2694.58   6.743    210
   2692.02   6.736    242
   2690.55   6.733    131
   2683.59   6.715    161
   2681.76   6.711    188
   2676.51   6.698    114
   2674.93   6.694    105
   2673.71   6.691     84
   2668.46   6.677     55
   2666.75   6.673     58
   2662.84   6.663    206
   2661.01   6.659    145
   2655.40   6.645    146
   2653.81   6.641    114
   1506.47   3.770   1000
   1497.19   3.747     48

in CDCl3