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1-(1,2,2-Trimethylpropyl)benzene synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 62 percent / ZnCl2 / 1,2-dichloro-ethane / 2.5 h / 20 °C
2: 1.) s-BuLi / 1.) THF, hexane, 2.) -78 deg C, 30 min then 20 deg C, 30 min

References:

Krief, Alain;Clarembeau, M.;Barbeaux, Ph. [Journal of the Chemical Society. Chemical communications,1986,# 6,p. 457 - 458]