[1,1'-Binaphthalene]-2-acetic acid, methyl ester synthesis

5synthesis methods

Product Name:[1,1'-Binaphthalene]-2-acetic acid, methyl ester
CAS Number:1329490-10-9
Molecular formula:C23H18O2
Molecular Weight:326.39

13922-41-3 Synthesis

13922-41-3
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[1,1'-Binaphthalene]-2-acetic acid, methyl ester

1329490-10-9
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate
2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane
3: ethanol; water
4: potassium hydroxide / ethanol
5: hydrogenchloride

References:

Kim, Jinho;Ohk, Youhwa;Park, Sae Hume;Jung, Yousung;Chang, Sukbok [Chemistry - An Asian Journal,2011,vol. 6,# 8,p. 2040 - 2047]

2586-62-1 Synthesis