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[1,1'-Biphenyl]-3-carboxaldehyde, 4'-ethenyl- synthesis

2synthesis methods
2039-82-9 Synthesis
4-Bromostyrene

2039-82-9
265 suppliers
$10.00/1g

Zinc, bis[3-(diethoxymethyl)phenyl]-

1256169-23-9
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[1,1'-Biphenyl]-3-carboxaldehyde, 4'-ethenyl-

84022-87-7
2 suppliers
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Yield:84022-87-7 93%

Reaction Conditions:

with dichloro{bis[1-(dicyclohexylphosphanyl)piperidine]}palladium(II) in tetrahydrofuran;1-methyl-pyrrolidin-2-one at 100; for 0.0833333 h;In air;Negishi cross-coupling reaction;

References:

Bolliger, Jeanne L.;Frech, Christian M. [Chemistry - A European Journal,2010,vol. 16,# 36,p. 11072 - 11081] Location in patent:experimental part