1-(1-cycloprop-2-enyl)-2-methyl-benzene synthesis
- Product Name:1-(1-cycloprop-2-enyl)-2-methyl-benzene
- CAS Number:65051-83-4
- Molecular formula:C10H10
- Molecular Weight:130.19
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 92 percent / aq. NaOH; cetrimide / 30 h / 35 - 40 °C
2: 85 percent / EtMgBr; Ti(i-PrO)4 / diethyl ether / 1.67 h / 20 °C
3: 79 percent / t-BuOK / dimethylsulfoxide / 10 h / 20 °C
References:
Rubin, Michael;Gevorgyan, Vladimir [Synthesis,2004,# 5,p. 796 - 800]
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