1,16-Hexadecanediamine synthesis

4synthesis methods

Product Name:1,16-Hexadecanediamine
CAS Number:929-94-2
Molecular formula:C16H36N2
Molecular Weight:256.47

1,16-Hexadecanediol, 1,16-bis(4-methylbenzenesulfonate)

73992-43-5
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929-94-2
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Yield:929-94-2 55%

Reaction Conditions:

Stage #1: hexadecane-1,16-diyl bis(4-methylbenzenesulfonate)with sodium azide in N,N-dimethyl-formamide at 60; for 9 h;
Stage #2: with triphenylphosphine in tetrahydrofuran;water at 20; for 12 h;Further stages.;

References:

Muranaka, Kazuhiro;Sano, Akiko;Ichikawa, Satoshi;Matsuda, Akira [Bioorganic and Medicinal Chemistry,2008,vol. 16,# 11,p. 5862 - 5870]

7735-42-4 Synthesis

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50602-69-2
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References

505-54-4
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$5.00/100mg

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References