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ChemicalBook CAS DataBase List (1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YL)-HYDRAZINE

(1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YL)-HYDRAZINE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 91 percent / Br2; 1,2-bis(diphenylphosphino)ethane / CH2Cl2 / -15 - 20 °C
2: fuming NH2NH2 / 0.5 h / sonication

References:

Braslau, Rebecca;Naik, Neeta;Zipse, Hendrik [Journal of the American Chemical Society,2000,vol. 122,# 35,p. 8421 - 8434]