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ChemicalBook CAS DataBase List 1,2,3,4-tetramethoxy-5-allylbenzene

1,2,3,4-tetramethoxy-5-allylbenzene synthesis

5synthesis methods
2103-57-3 Synthesis
2,3,4-Trimethoxybenzaldehyde

2103-57-3
499 suppliers
$9.00/10g

1,2,3,4-tetramethoxy-5-allylbenzene

15361-99-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: formic acid; dihydrogen peroxide / dichloromethane; water / 20 °C / Reflux
2: potassium carbonate / acetone / Reflux
3: diethylaluminium chloride / hexane / 1 h / 0 °C / Inert atmosphere
4: potassium carbonate / acetone / 20 °C

References:

Bochicchio, Antonella;Cefola, Rossella;Choppin, Sabine;Colobert, Fran?oise;Di Noia, Maria Antonietta;Funicello, Maria;Hanquet, Gilles;Pisano, Isabella;Todisco, Simona;Chiummiento, Lucia [Tetrahedron Letters,2016,vol. 57,# 36,p. 4053 - 4055]