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1,2,3,4-Tetraphenyl-1,3-butadiene synthesis

7synthesis methods
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Yield:103-30-0 88.7 %Chromat. ,645-49-8 9.2 %Chromat. ,806-71-3 1.1 %Chromat. ,103-29-7 1.0 %Chromat.

Reaction Conditions:

with Pd(PCy2CH2CH2PCy2)(OTf)2;hydrogen in methanol at 48.84; under 3040.2 Torr; for 1 h;Inert atmosphere;

References:

Lopez-Serrano, Joaquin;Duckett, Simon B.;Dunne, John P.;Godard, Cyril;Whitwood, Adrian C. [Dalton Transactions,2008,# 32,p. 4270 - 4281] Location in patent:body text