1-(2,3-dihydro-1H-isoindol-5-yl)-Ethanone synthesis
- Product Name:1-(2,3-dihydro-1H-isoindol-5-yl)-Ethanone
- CAS Number:905274-46-6
- Molecular formula:C10H11NO
- Molecular Weight:161.2
850877-60-0
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Yield:-
Reaction Conditions:
with hydrogenchloride in 1,4-dioxane;water at 20; for 16 h;
Steps:
51.2 1-(isoindolin-5-yl)ethan-1-one 51c
To a mixture of 51b (50 mg, 191.34 umol) in DCM (3 mL) was added dioxane/HCl (IN, lmL). The reaction was stirred at room temperature for 16h. The mixture was concentrated to give crude 51c, the crude product was used to the next step directly without purification.
References:
WO2021/158626,2021,A1 Location in patent:Page/Page column 120
201940-08-1
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