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1,2,3-Thiadiazole-4-carbothioamide, 5-amino- synthesis

5synthesis methods
1,2,3-Thiadiazole-4-carbonitrile, 5-amino-

41266-81-3
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1,2,3-Thiadiazole-4-carbothioamide, 5-amino-

100097-66-3
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Yield:100097-66-3 98%

Reaction Conditions:

with hydrogen sulfide;triethylamine in chloroform at 0 - 5; for 0.5 h;

References:

Dankova, E. F.;Bakulev, V. A.;Kolobov, M. Yu.;Shishkina, V. I.;Yasman, Ya. B.;Lebedev, A. T. [Chemistry of Heterocyclic Compounds,1988,vol. 24,# 9,p. 1051 - 1055][Khimiya Geterotsiklicheskikh Soedinenii,1988,# 9,p. 1269 - 1273]