1,2,4,6-Tetra-O-acetyl-3-deoxy-D-glucopyranose synthesis
- Product Name:1,2,4,6-Tetra-O-acetyl-3-deoxy-D-glucopyranose
- CAS Number:5040-09-5
- Molecular formula:C14H20O9
- Molecular Weight:332.3
![3-(2,2-dimethyl-1,3-dioxolan-4-yl)-7,7-dimethyl-2,6,8-trioxabicyclo[3.3.0]octane](/CAS/GIF/4613-62-1.gif)
Yield:5040-09-5 20%
Reaction Conditions:
Stage #1: 3-deoxy-1,2;5,6-di-O-isopropylidene-α-D-glucofuranosidewith trifluoroacetic acid in water;acetic acid at 20;
Stage #2: acetic anhydridewith pyridineFurther stages.;
References:
Danac, Ramona;Ball, Lucy;Gurr, Sarah J.;Fairbanks, Antony J. [Carbohydrate Research,2008,vol. 343,# 6,p. 1012 - 1022]
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