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ChemicalBook CAS DataBase List 1,2-BIS[(DIMETHYLAMINO)DIMETHYLSILYL]ETHANE
91166-50-6

1,2-BIS[(DIMETHYLAMINO)DIMETHYLSILYL]ETHANE synthesis

1synthesis methods
the reagent is prepared as a colorless liquid in 90% yield by treating commercially available bis(chlorodimethylsilyl) ethane with 5 equiv of dimethylamine in ether at 0°C for 5 h.
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Yield:91166-50-6 90%

Reaction Conditions:

in diethyl ether at 0; for 5 h;

References:

Guggenheim, Thomas L. [Tetrahedron Letters,1984,vol. 25,# 12,p. 1253 - 1254]

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