1-(2-bromophenyl)cyclopropan-1-ol synthesis

3synthesis methods

Product Name:1-(2-bromophenyl)cyclopropan-1-ol
CAS Number:1186503-77-4
Molecular formula:C9H9BrO
Molecular Weight:213.07

75-11-6
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Benzene, 1-bromo-2-[1-[(trimethylsilyl)oxy]ethenyl]-

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1186503-77-4
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Yield:1186503-77-4 52%

Reaction Conditions:

Stage #1: diiodomethane;o-bromoacetophenone trimethylsilyl enol etherwith diethylzinc in diethyl ether;hexane at 0; for 4 h;Reflux;
Stage #2: with potassium carbonate in methanol at 20; for 0.5 h;

References:

Wang, Yi-Feng;Chiba, Shunsuke [Journal of the American Chemical Society,2009,vol. 131,# 35,p. 12570 - 12572] Location in patent:supporting information; experimental part

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References

2142-69-0 Synthesis

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References