1,2-Dimethylhydrazine Dihydrochloride synthesis
- Product Name:1,2-Dimethylhydrazine Dihydrochloride
- CAS Number:306-37-6
- Molecular formula:C2H10Cl2N2
- Molecular Weight:133.02
74-89-5
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306-37-6
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Yield:-
Reaction Conditions:
Stage #1: methylaminewith triethylamine in dichloromethane; for 0.25 h;
Stage #2: with bis(trichloromethyl) carbonate in dichloromethane at -5 - 0; for 1 h;
References:
Baruah, Kalpita;Sahariah, Biswajit;Sakpal, Sushil S.;Deka, Jugal Kishore Rai;Bar, Arun Kumar;Bagchi, Sayan;Sarma, Bani Kanta [Organic Letters,2021,vol. 23,# 13,p. 4949 - 4954] Location in patent:supporting information