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1,2-Diphenyl-1-(dimethylamino)ethane synthesis

9synthesis methods
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Yield:6319-84-2 89%

Reaction Conditions:

Stage #1: N,N-dimethylbenzamidewith bis(triphenylphosphine)carbonyliridium(I) chloride;1,1,3,3-Tetramethyldisiloxane in dichloromethane at 20; for 0.333333 h;
Stage #2: benzylmagnesium chloride at -78 - 20; for 4 h;Catalytic behavior;Solvent;

References:

Xie, Lan-Gui;Dixon, Darren J. [Chemical Science,2017,vol. 8,# 11,p. 7492 - 7497]