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ChemicalBook CAS DataBase List 1,2-O-Cyclohexylidene-myo-inositol
6763-47-9

1,2-O-Cyclohexylidene-myo-inositol synthesis

4synthesis methods
-

Yield:6763-47-9 98%

Reaction Conditions:

Stage #1: D-myo-inositol;cyclohexanonewith toluene-4-sulfonic acid in N,N-dimethyl-formamide;toluene at 122 - 136; for 10 h;Condensation;
Stage #2: with ethanol;toluene-4-sulfonic acid at 20; for 48 h;alcoholysis;

References:

Morisaki, Kazuo;Ozaki, Shoichiro [Carbohydrate Research,1996,vol. 286,p. 123 - 138]